N-(己烷-2-亚基氨基)-2,4-二硝基苯胺合成路线 （共 15 条）
反应条件
1: 82 percent / butyl-lithium / hexane; tetrahydrofuran / 0 °C 2: 79 percent / di-isobutylaluminum hydride / toluene / 48 h / Heating 3: 85percent m-chloroperbenzoic acid / CH2Cl2 / 1.5 h / -23 °C View Scheme
参考文献
Ager, David J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 195 - 204
反应条件
1: 1.) butyl-lithium, 2.) TMEDA / 1.) hexane, THF, 0 deg C, 1.5 h, 2.) hexane, THF, 12 h 2: 85percent m-chloroperbenzoic acid / CH2Cl2 / 1.5 h / -23 °C View Scheme
参考文献
Ager, David J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 195 - 204
参考文献
Eglinton et al.
Journal of the Chemical Society, 1952 , p. 2873,2880
反应条件
hydrogenchloride; ammonium cerium(IV) nitrate; nitric acid 1.) 12 h; Yield given. Multistep reaction;
参考文献
Mathur, Dwarka, L.; Agarwal, Anupma; Banerji, Kalyan K.
Journal of the Indian Chemical Society, 1985 , vol. 62, # 7 p. 519 - 522
反应条件
Yield given. Multistep reaction;
参考文献
Ager, David J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 195 - 204
