2-苯基萘-1,4-二酮合成路线 （共 49 条）
反应条件
dipotassium peroxodisulfate; iron(III) sulphate hydrate; oxygen; potassium carbonate in water
T=70°C; 24 h; Green chemistry;
参考文献
Deb, Arghya; Agasti, Soumitra; Saboo, Tapish; Maiti, Debabrata
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 4 p. 705 - 710
反应条件
manganese(III) sulphate; sulfuric acid in acetonitrile
T=50°C; 3 h;
参考文献
Bhatt, M. Vivekananda; Periasamy, Mariappan
Tetrahedron, 1994 , vol. 50, # 11 p. 3575 - 3586
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in acetonitrile
T=20°C;
参考文献
Patil, Pravin; Nimonkar, Abhay; Akamanchi, Krishnacharya G.
Journal of Organic Chemistry, 2014 , vol. 79, # 5 p. 2331 - 2336
反应条件
acetic acid
T=80°C; Erwaermen des Reaktionsgemisches mit CrO3 in Wasser;
参考文献
Fieser et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 3177
反应条件
1: 65 percent / 2,6-lutidine, DMAP / CH2Cl2 / 3 h / 23 °C
2: 73 percent / NMP / Pd2(dba)3*dba / 16 h / 23 °C
View Scheme
参考文献
Echavarren, Antonio M.; Frutos, Oscar de; Tamayo, Nuria; Noheda, Pedro; Calle, Paloma
Journal of Organic Chemistry, 1997 , vol. 62, p. 4524 - 4527
反应条件
Cu(BF4)2*6H2O; bis(1,2-diphenylphosphino)benzene; palladium (II) 2,4-pentanedionate in 1,4-dioxane; water
T=20°C; 18 h;
参考文献
Molina, Maria Teresa; Navarro, Cristina; Moreno, Ana; Csaky, Aurelio G.
Organic Letters, 2009 , vol. 11, # 21 p. 4938 - 4941
反应条件
potassium dihydrogenphosphate; K2lt;S2O7(NO)gt; in methanol; water
20 h; Ambient temperature;
参考文献
Watanabe; Hisamatsu; Hotokezaka; Furukawa
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 7 p. 2810 - 2820
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in water; benzene
Suzuki coupling; 3 h; Heating;
参考文献
Best, Wayne M.; Sims, Colette G.; Winslade, Merilyn
Australian Journal of Chemistry, 2001 , vol. 54, # 6 p. 401 - 404
反应条件
lithium chloropalladite in acetonitrile
24 h; Ambient temperature;
参考文献
Singh; Rohtagi; Khanna
Synthetic Communications, 1992 , vol. 22, # 7 p. 987 - 993
反应条件
1: in benzene
T=40°C; 22 h; Inert atmosphere;
2: With ammonium cerium (IV) nitrate in diethyl ether; benzene
T=20°C; 3 h; Inert atmosphere;
参考文献
Wu, Chunrui; Berbasov, Dmytro O.; Wulff, William D.
Journal of Organic Chemistry, 2010 , vol. 75, # 13 p. 4441 - 4452
