2-苯基萘-1,4-二酮合成路线 （共 49 条）
反应条件
[iron tetracarbonyl]
2.) CH3CN, 100 deg C, 6 h; Yield given. Multistep reaction;
参考文献
Liebeskind, Lanny S.; Baysdom, Sherrol L.; South, Mivhael S.
Journal of the American Chemical Society, 1980 , vol. 102, # 24 p. 7397 - 7398
反应条件
dipotassium peroxodisulfate; iron(III) sulphate hydrate; oxygen; potassium carbonate in water
T=70°C; 24 h; Green chemistry;
参考文献
Deb, Arghya; Agasti, Soumitra; Saboo, Tapish; Maiti, Debabrata
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 4 p. 705 - 710
反应条件
ethanol; sodium acetate
参考文献
Kvalnes
Journal of the American Chemical Society, 1934 , vol. 56, p. 2478,2479
反应条件
in acetonitrile
2 h; Irradiation;
参考文献
Thaplial, Prakash Chander
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1998 , vol. 37, # 5 p. 477 - 479
反应条件
1: 1.) dimethyl sulfoxide, 2.) 10percent NaOH / 1.) 140-145 deg C, 15 min, 2.) ethanol, water, reflux, 15 min
2: 64 percent / potassium dichromate, sulfuric acid / diethyl ether / 2 h
View Scheme
参考文献
Janowski, Wit K.; Prager, Rolf H.
Australian Journal of Chemistry, 1985 , vol. 38, # 6 p. 921 - 929
反应条件
1: 28 percent / dimethyl sulfoxide / 0.25 h / 140 - 145 °C
2: 90 percent / 10percent NaOH / ethanol; H2O / 15 h / Heating
3: 64 percent / potassium dichromate, sulfuric acid / diethyl ether / 2 h
View Scheme
参考文献
Janowski, Wit K.; Prager, Rolf H.
Australian Journal of Chemistry, 1985 , vol. 38, # 6 p. 921 - 929
反应条件
1: 10percent NaOH / ethanol; H2O / 0.25 h / Heating
2: 64 percent / potassium dichromate, sulfuric acid / diethyl ether / 2 h
View Scheme
参考文献
Janowski, Wit K.; Prager, Rolf H.
Australian Journal of Chemistry, 1985 , vol. 38, # 6 p. 921 - 929
反应条件
1: 1) lithium N-isopropylcyclohexylamide / 1) THF, hexane, -78 deg C, 1 h; 2) THF, -20 deg C, then room temp., overnight
2: 26 percent / K2<S2O7(NO)>, KH2PO4 / methanol; H2O / 20 h / Ambient temperature
View Scheme
参考文献
Watanabe; Hisamatsu; Hotokezaka; Furukawa
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 7 p. 2810 - 2820
反应条件
potassium dihydrogenphosphate; Fremy’s salt in methanol
参考文献
Kipping,C. et al.
Journal fuer Praktische Chemie (Leipzig), 1973 , vol. 315, # 5 p. 887 - 894
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide
T=85°C; Product distribution; Further Variations:ReagentsSolvents;
参考文献
Davies; Johnson; Harrity
Journal of Organic Chemistry, 2001 , vol. 66, # 10 p. 3525 - 3532
