1-氯-1-甲基硅杂环丁烷合成路线 （共 15 条）
反应条件
magnesium; ethylene dibromide in dibutyl diglyme T=20 - 95°C; Grignard Reaction; 2 h;
参考文献
STARFIRE SYSTEMS, INC.
Patent: WO2008/33980 A2, 2008 ;
Location in patent: Page/Page column 8-9 ;
反应条件
magnesium in diethyl ether 48 h;
参考文献
Auner, N.; Grobe, J.
Journal of Organometallic Chemistry, 1980 , vol. 188, # 1 p. 25 - 52
反应条件
magnesium in tetrahydrofuran
参考文献
Dow Corning Asia, Ltd.
Patent: US5502229 A1, 1996 ;
反应条件
tert.-butyl lithium in pentane T=-20°C;
参考文献
Auner, N.
Journal of Organometallic Chemistry, 1987 , vol. 336, p. 83 - 104
反应条件
magnesium; ethylene dibromide in tetrahydrofuran T=0°C;
参考文献
Ushakov; Fedorova
Russian Chemical Bulletin, 1996 , vol. 45, # 4 p. 901 - 910
反应条件
in diethyl ether T=-78 - 20°C;
参考文献
Journal of Organometallic Chemistry, , vol. 188, # 1 p. 25 - 52
反应条件
in diethyl ether T=20°C; 3 h;
参考文献
Journal of Organometallic Chemistry, , vol. 188, # 1 p. 25 - 52
反应条件
1.5 h; Ambient temperature; Further byproducts given;
参考文献
Ducker, Graham E.; Tipping, Anthony E.
Journal of Fluorine Chemistry, 1994 , vol. 67, # 2 p. 129 - 136
反应条件
lithium aluminium tetrahydride in anhydrous butyl ether
T=-5 - 5°C;
参考文献
Auner, N.; Grobe, J.
Journal of Organometallic Chemistry, 1980 , vol. 188, # 1 p. 25 - 52
