4-氧代环己烷-1-醇对甲苯磺酸酯合成路线 （共 8 条）
反应条件
lithium bromide in acetone Heating;
参考文献
Mihovilovic; Chen; Wang; Kyte; Rochon; Kayser; Stewart
Journal of Organic Chemistry, 2001 , vol. 66, # 3 p. 733 - 738
反应条件
acetic acid; pyridinium chlorochromate in chloroform
T=20°C; 66 h;
参考文献
Rotstein, David Mark; Melville, Chris Richard
Patent: US2008/249087 A1, 2008 ;
Location in patent: Page/Page column 30-31 ;
US 20080249087 A1
反应条件
MnCl2∙4H2O; water; 3-chloro-benzenecarboperoxoic acid; Ru(4,4′,4''-tri-t-butyl-2,2′;6,2″-terpyridine)Cl3 in acetonitrile
T=0 - 20°C; 4 h; chemoselective reaction;
参考文献
Kamijo, Shin; Amaoka, Yuuki; Inoue, Masayuki
Synthesis, 2010 , # 14 art. no. E27210SS, p. 2475 - 2489
反应条件
1: pyridine
2: CrO3 / acetone; acetic acid / 0.5 h / 15 - 20 °C
View Scheme
参考文献
Davies, Ann P.; Legon, A. C.; Millen, D. J.; Roberts, A. J.
Journal of Molecular Structure, 1984 , vol. 112, p. 9 - 18
反应条件
1: sodium tetrahydroborate / methanol-d1 / 0 °C
2: toluene-4-sulfonic acid / water / |Heating
3: pyridine / 20 °C
View Scheme
参考文献
De Vos, Nils; Maton, Cedric; De Vreese, Peter; Brooks, Neil R.; Binnemans, Koen; Stevens, Christian V.
European Journal of Organic Chemistry, 2013 , # 18 p. 3741 - 3750
反应条件
1: toluene-4-sulfonic acid / water / |Heating
2: pyridine / 20 °C
View Scheme
参考文献
De Vos, Nils; Maton, Cedric; De Vreese, Peter; Brooks, Neil R.; Binnemans, Koen; Stevens, Christian V.
European Journal of Organic Chemistry, 2013 , # 18 p. 3741 - 3750
参考文献
De Vos, Nils; Maton, Cedric; De Vreese, Peter; Brooks, Neil R.; Binnemans, Koen; Stevens, Christian V.
European Journal of Organic Chemistry, 2013 , # 18 p. 3741 - 3750
反应条件
1: pyridine
2: CrO3 / acetone; acetic acid / 0.5 h / 15 - 20 °C
View Scheme
参考文献
Davies, Ann P.; Legon, A. C.; Millen, D. J.; Roberts, A. J.
Journal of Molecular Structure, 1984 , vol. 112, p. 9 - 18
