1,2,2,2-四氟乙基三氟甲醚合成路线 (共 7 条)
反应条件
potassium hydroxide T=230°C;
参考文献
E. I. du Pont de Nemours and Company
Patent: US6905630 B2, 2005 ;
Location in patent: Page/Page column 5 ;
反应条件
bromine trifluoride T=40 - 45°C; Fluorination; 5 h;
参考文献
Hudlicky, Tomas; Duan, Caiming; Reed, Josephine W.; Yan, Fengyang; Hudlicky, Milos; Endoma, Mary Ann; Eger II, Edmond I.
Journal of Fluorine Chemistry, 2000 , vol. 102, # 1-2 p. 363 - 367
反应条件
fluorine; NAF Further byproducts given;
参考文献
Sekiya, Akira; Ueda, Kunimasa
Chemistry Letters, 1990 , # 4 p. 609 - 612
反应条件
potassium fluoride; formamide
参考文献
Gubanov,V.A. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1964 , vol. 34, p. 2802 - 2803,2825 - 2826
反应条件
fluorine; NAF 20 h; -111 deg C to 20 deg C;
参考文献
Sekiya, Akira; Ueda, Kunimasa
Chemistry Letters, 1990 , # 4 p. 609 - 612
反应条件
(electrochemical fluorination);
参考文献
Berenblit,V.V. et al.
Journal of Organic Chemistry USSR (English Translation), 1976 , vol. 12, p. 765 - 768
Zhurnal Organicheskoi Khimii, 1976 , vol. 12, p. 767 - 770
反应条件
in monofluoro-trichloromethane T=-105°C; competition with ClFC=CFCl and FHC=CF2, relative addition rates and orientation ratios; Rate constantProduct distribution;
参考文献
Navarrini, W.; Russo, A.; Tortelli, V.
Journal of Organic Chemistry, 1995 , vol. 60, # 20 p. 6441 - 6443