3-(n-苄胺)丙酸甲酯合成路线 (共 24 条)
反应条件
1: 91 percent / K2CO3 / CHCl3 / 7.5 h / Heating 2: 1) C2H5OK, 2) HCl / 1) ethanol, xylene, reflux, 16 h; 2) ethanol. 3: 92 percent / K2CO3, sodium dihydridobis(2-methoxyethoxo)aluminate / benzene; toluene View Scheme
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 51, # 9 p. 2034 - 2049
反应条件
lithium aluminium tetrahydride
参考文献
Barco, Achille; Benetti, Simonetta; Risi, Carmela De; Pollini, Gian P.; Romagnoli, Romeo; Zanirato, Vinicio
Tetrahedron Letters, 1994 , vol. 35, # 49 p. 9293 - 9296
反应条件
hydrogen in methanol P=760 Torr;
参考文献
Lima, Paulo G.; Sequeira, Lucia C.; Costa, Paulo R.R.
Tetrahedron Letters, 2001 , vol. 42, # 21 p. 3525 - 3527
反应条件
T=100 - 110°C; 168 h; sealed tube;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 9 p. 2525 - 2530
反应条件
T=100 - 110°C; 168 h; sealed tube;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 9 p. 2525 - 2530
反应条件
T=100 - 110°C; 168 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 9 p. 2525 - 2530
反应条件
1.1: triethylamine / dichloromethane / 0 °C 1.2: 12 h / 0 - 20 °C 2.1: sodium hydroxide / water; methanol / 2 h / 20 °C View Scheme
参考文献
Groselj, Uros; Podlogar, Anja; Novak, Ana; Dahmann, Georg; Golobic, Amalija; Stanovnik, Branko; Svete, Jurij
Synthesis (Germany), 2013 , vol. 45, # 5 art. no. SS-2012-Z0909-OP, p. 639 - 650
反应条件
potassium carbonate in chloroform 7.5 h; Heating;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 51, # 9 p. 2034 - 2049
反应条件
T=100 - 110°C; 168 h; sealed tube;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 9 p. 2525 - 2530
反应条件
T=100 - 110°C; 168 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 9 p. 2525 - 2530