2,3-二氢-3-甲基-2-亚甲基苯并噻唑合成路线 (共 9 条)
参考文献
Bayer Aktiengesellschaft
Patent: US4349670 A1, 1982 ;
反应条件
TMG; sodium hydride in Petroleum ether
参考文献
Owen,J.R.
Tetrahedron Letters, 1969 , # 32 p. 2709 - 2712
反应条件
sodium hydride in tetrahydrofuran
参考文献
Quast, Helmut; Ivanova, Svetlana; Peters, Eva-Maria; Peters, Karl; Von Schnering, Hans Georg
Liebigs Annales, 1996 , # 10 p. 1541 - 1549
反应条件
1: methanol
2: aq. HCl / 4.5 h / Heating
View Scheme
参考文献
Boberg,F. et al.
Justus Liebigs Annalen der Chemie, 1976 , p. 2267 - 2271
参考文献
Quast, Helmut; Ach, Manfred; Kindermann, Markus K.; Rademacher, Paul; Schindler, Michael
Chemische Berichte, 1993 , vol. 126, # 2 p. 503 - 516
反应条件
hydrogenchloride
4.5 h; Heating;
参考文献
Boberg,F. et al.
Justus Liebigs Annalen der Chemie, 1976 , p. 2267 - 2271
反应条件
T=300°C; relative percentage of isolated volatile products of thermolysis; Product distributionMechanism;
参考文献
Al'perovich, M. A.; Khesin, V. G.; Raikhina, R. D.; Medvedeva, T. D.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1981 , vol. 17, # 12 p. 1182 - 1187
Khimiya Geterotsiklicheskikh Soedinenii, 1981 , vol. 17, # 12 p. 1620 - 1625
反应条件
T=300°C; P=735.5 Torr; relative percentage of isolated volatile product of thermolysis; Product distribution;
参考文献
Khesin, V. G.; Al'perovich, M. A.; Abramenko, P. I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1981 , vol. 17, # 12 p. 1187 - 1192
Khimiya Geterotsiklicheskikh Soedinenii, 1981 , vol. 17, # 12 p. 1626 - 1630
反应条件
T=300°C; relative percentage of isolated volatile products of thermolysis; Product distributionMechanism;
参考文献
Al'perovich, M. A.; Khesin, V. G.; Raikhina, R. D.; Medvedeva, T. D.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1981 , vol. 17, # 12 p. 1182 - 1187
Khimiya Geterotsiklicheskikh Soedinenii, 1981 , vol. 17, # 12 p. 1620 - 1625