2-(2,2,2-三氟乙氧基)乙醇合成路线 （共 7 条）
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 0.75 h;
参考文献
Chugai Seiyaku Kabushiki Kaisha
Patent: US6645951 B1, 2003 ;
Location in patent: Page/Page column 192 ;
反应条件
sodium hydroxide in bis [2-(2-methoxyethoxy)ethyl] ether T=150°C; 4 h; Product distribution / selectivity;
参考文献
SOLVAY SPECIALTY POLYMERS ITALY S.p.A.; TORTELLI, Vito; WLASSICS, Ivan; MONZANI, Cristiano; KENT, Bradley Lane; VENERONI, Alessandro
Patent: WO2012/160135 A1, 2012 ;
Location in patent: Page/Page column 16-17 ;
反应条件
magnesium bromide in diethyl ether
参考文献
Minnesota Mining and Manufacturing Company
Patent: US5157159 A1, 1992 ;
反应条件
triethylamine T=95°C; 16 h; Yields of byproduct given;
参考文献
Heilmann, S. M.; Drtina, G. J.; Janulis, E. P.; Krepski, L. R.; Rasmussen, J. K.; et al.
Journal of Fluorine Chemistry, 1992 , vol. 59, # 3 p. 387 - 396
参考文献
Journal of the American Chemical Society, , vol. 79, p. 6533,6534,6536
反应条件
phosphorus pentachloride
参考文献
Brey; Tarrant
Journal of the American Chemical Society, 1957 , vol. 79, p. 6533,6534,6536
