1,1-二苯基-3,3-二甲基-1-丁烯合成路线 （共 20 条）
反应条件
in dimethyl sulfoxide T=35 - 40°C; 12 h; Irradiation;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.
Organometallics, 1988 , vol. 7, p. 696 - 702
反应条件
1: diphenylmethyl diethyl phosphate With n-butyllithium in tetrahydrofuran T=20°C; 1 h; 2: pivalaldehyde in tetrahydrofuran 2 h;
参考文献
Varela, Jesus A.; Pena, Diego; Goldfuss, Bernd; Polborn, Kurt; Knochel, Paul
Organic Letters, 2001 , vol. 3, # 15 p. 2395 - 2398
反应条件
Ph2CCHSO2Ph in dimethyl sulfoxide Irradiation (UV/VIS); mercurial and organic compound dissolved in nitrogen purged solvent, irradn. (350-nm Rayonet photoreactor, 35-40°C, 20 h);; mixt. poured into water; extn. with benzene; ext. washed (aq. Na2S2O3), dried (Na2SO4) and concd. (vacuum); yield detd. by GLC;;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.; Pla-Dalmau, Anna; Khanna, Rajive K.
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3530 - 3538
反应条件
in benzene T=35 - 40°C; 18 h;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.
Organometallics, 1988 , vol. 7, p. 696 - 702
反应条件
potassium phosphate; PCy3∙HBF4; bis(1,5-cyclooctadiene)nickel (0) in tetrahydrofuran T=75°C; Suzuki-Miyaura coupling; 18 h;
参考文献
Hansen, Anders L.; Ebran, Jean-Philippe; Gogsig, Thomas M.; Skrydstrup, Troels
Journal of Organic Chemistry, 2007 , vol. 72, # 17 p. 6464 - 6472
反应条件
in dimethyl sulfoxide T=35 - 40°C; 24 h; Irradiation;
参考文献
Russell, Glen A.; Tashtoush, Hasan; Ngoviwatchai, Preecha
Journal of the American Chemical Society, 1984 , vol. 106, # 16 p. 4622 - 4623
反应条件
1: phenyl-magnesium bromide With zinc(II) chloride in tetrahydrofuran; acetonitrile T=0°C; 0.166667 h; Inert atmosphere; 2: 2-methyl-2-iodopropane; phenylacetylene With bis(acetylacetonate)nickel(II); 1,4-di(diphenylphosphino)-butane in tetrahydrofuran; acetonitrile T=0 - 25°C; Inert atmosphere;
参考文献
Terao, Jun; Bando, Fumiaki; Kambe, Nobuaki
Chemical Communications, 2009 , # 47 p. 7336 - 7338
反应条件
in dimethyl sulfoxide T=35 - 40°C; 14 h; Irradiation;
参考文献
Russell, Glen A.; Tashtoush, Hasan; Ngoviwatchai, Preecha
Journal of the American Chemical Society, 1984 , vol. 106, # 16 p. 4622 - 4623
反应条件
tert.-butyl lithium in benzene Irradiation (UV/VIS); mixt. of mercurial and organometallic compd. (1 equiv) is irradiated in nitrogen-purged solvent in Pyrex tube with 350-nm Rayonet photoreactor for 24 h; mixt. is poured into water, extd., extract is washed twice with aq. sodium thiosulfate, dried over anhyd. Na2SO4, concd.; GLC;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.
Organometallics, 1988 , vol. 7, p. 696 - 702
反应条件
in benzene T=35 - 40°C; 24 h; Irradiation;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.; Pla-Dalmau, Anna; Khanna, Rajive K.
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3530 - 3538
