1,1-二苯基-3,3-二甲基-1-丁烯合成路线 （共 20 条）
反应条件
in dimethyl sulfoxide T=35 - 40°C; 20 h; Irradiation;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.; Pla-Dalmau, Anna; Khanna, Rajive K.
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3530 - 3538
反应条件
tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0) in diethyl ether; toluene T=20°C; 2 h;
参考文献
Kambe, Nobuaki; Moriwaki, Yuusuke; Fujii, Yuuki; Iwasaki, Takanori; Terao, Jun
Organic Letters, 2011 , vol. 13, # 17 p. 4656 - 4659
参考文献
Adam,W. et al.
Journal of the American Chemical Society, 1972 , vol. 94, p. 2000 - 2006
反应条件
1: 100 percent / dimethylsulfoxide / 12 h / 35 - 40 °C / Irradiation 2: 88 percent / dimethylsulfoxide / 24 h / 35 - 40 °C / Irradiation View Scheme
参考文献
Russell, Glen A.; Tashtoush, Hasan; Ngoviwatchai, Preecha
Journal of the American Chemical Society, 1984 , vol. 106, # 16 p. 4622 - 4623
反应条件
in tetrahydrofuran; benzene Irradiation (UV/VIS); mixt. of mercurial and organometallic compd. (2 equiv) is irradiated in nitrogen-purged solvent in Pyrex tube with 350-nm Rayonet photoreactor for 5 h; mixt. is poured into water, extd., extract is washed twice with aq. sodium thiosulfate, dried over anhyd. Na2SO4, concd.; GLC;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.
Organometallics, 1988 , vol. 7, p. 696 - 702
反应条件
in tetrahydrofuran Irradiation (UV/VIS); mercurial and organometallic compound is irradiated in nitrogen-purged solvent in Pyrex tube with 350-nm Rayonet photoreactor for 24 h; NMR;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.
Organometallics, 1988 , vol. 7, p. 696 - 702
反应条件
(i) toluene, (ii) H2O; Multistep reaction;
参考文献
Eisch,J.J.; Amtmann,R.
Journal of Organic Chemistry, 1972 , vol. 37, p. 3410 - 3415
反应条件
in dimethyl sulfoxide T=35 - 40°C; 90 h; Irradiationother reagent, other time, various moles ratio; Product distribution;
参考文献
Russell, Glen A.; Khanna, Rajive K.; Guo, Deliang
Journal of the Chemical Society, Chemical Communications, 1986 , # 8 p. 632 - 634
反应条件
monoaluminum phosphate in ethylene glycol dimethyl ether 1.5 h; Ambient temperatureother reagents; product selectivity; Product distributionMechanism;
参考文献
Campelo, Juan M.; Chakraborty, Rupak; Marinas, Jose M.
Synthetic Communications, 1996 , vol. 26, # 9 p. 1639 - 1650
反应条件
monoaluminum phosphate; zinc(II) tetrahydroborate in ethylene glycol dimethyl ether 1.5 h; Ambient temperatureother reagents; product selectivity; Product distribution;
参考文献
Campelo, Juan M.; Chakraborty, Rupak; Marinas, Jose M.
Synthetic Communications, 1996 , vol. 26, # 9 p. 1639 - 1650
