2-[亚硝基[3-(三氟甲基)苯基]氨基]-苯甲酸合成路线 （共 4 条）
反应条件
acetic anhydride; acetic acid; sodium nitrite T=0°C; 3 h;
参考文献
Ryu, Jaeyune; Shin, Kwangmin; Park, Sae Hume; Kim, Ji Young; Chang, Sukbok
Angewandte Chemie - International Edition, 2012 , vol. 51, # 39 p. 9904 - 9908
反应条件
1: triethylamine / dichloromethane / 5 h / 0 - 20 °C / |Inert atmosphere 2: [{(η5-C5Me5)RhCl}2(μ-Cl)2]; silver hexafluoroantimonate / 1,2-dichloro-ethane / 24 h / 85 °C 3: acetic acid; acetic anhydride; sodium nitrite / 3 h / 0 °C View Scheme
参考文献
Ryu, Jaeyune; Shin, Kwangmin; Park, Sae Hume; Kim, Ji Young; Chang, Sukbok
Angewandte Chemie - International Edition, 2012 , vol. 51, # 39 p. 9904 - 9908
反应条件
1: sodium azide; copper diacetate / methanol / 3 h / 55 °C 2: [{(η5-C5Me5)RhCl}2(μ-Cl)2]; silver hexafluoroantimonate / 1,2-dichloro-ethane / 24 h / 85 °C 3: acetic acid; acetic anhydride; sodium nitrite / 3 h / 0 °C View Scheme
参考文献
Ryu, Jaeyune; Shin, Kwangmin; Park, Sae Hume; Kim, Ji Young; Chang, Sukbok
Angewandte Chemie - International Edition, 2012 , vol. 51, # 39 p. 9904 - 9908
反应条件
1: [{(η5-C5Me5)RhCl}2(μ-Cl)2]; silver hexafluoroantimonate / 1,2-dichloro-ethane / 24 h / 85 °C 2: acetic acid; acetic anhydride; sodium nitrite / 3 h / 0 °C View Scheme
参考文献
Ryu, Jaeyune; Shin, Kwangmin; Park, Sae Hume; Kim, Ji Young; Chang, Sukbok
Angewandte Chemie - International Edition, 2012 , vol. 51, # 39 p. 9904 - 9908
