L-苯基丙氨酸对硝基苯胺合成路线 (共 16 条)
反应条件
methanol; acetyl chloride in dichloromethane T=20°C; 24 h;
参考文献
Journal of the American Chemical Society, , vol. 129, # 29 p. 8928 - 8929
反应条件
copper(l) iodide; potassium carbonate in toluene T=110°C; 24 h; Inert atmosphereSealed tube;
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 4 p. 692 - 696
反应条件
copper(l) iodide; potassium carbonate in toluene T=110°C; 24 h; Inert atmosphereSealed tube;
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 4 p. 692 - 696
反应条件
1.1: 1,1-carbonyldiimidazole / CH2Cl2 / 0.5 h / 20 °C 1.2: 1,8-diazabicyclo[5.4.0]undec-7-ene / CH2Cl2 / 20 h / 20 °C 2.1: acetyl chloride; methanol / CH2Cl2 / 24 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 129, # 29 p. 8928 - 8929
反应条件
1.1: 1,1-carbonyldiimidazole / CH2Cl2 / 0.5 h / 20 °C 1.2: 1,8-diazabicyclo[5.4.0]undec-7-ene / CH2Cl2 / 20 h / 20 °C 2.1: acetyl chloride; methanol / CH2Cl2 / 24 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 129, # 29 p. 8928 - 8929
反应条件
hydrogen bromide; acetic acid
参考文献
Chemical and pharmaceutical bulletin, , vol. 33, # 12 p. 5301 - 5309
反应条件
2: 25percent HBr, acetic acid View Scheme
参考文献
Chemical and pharmaceutical bulletin, , vol. 33, # 12 p. 5301 - 5309
反应条件
endopeptidase in various solvent(s) T=25°C; 1 h; pH=8.0; apparent rate of hydrolysis;
参考文献
Chemical and pharmaceutical bulletin, , vol. 34, # 1 p. 275 - 280
反应条件
1.1: 0.1 mol/l HCl / H2O / 0.5 h / 100 °C 1.2: 90 percent / H2O; CH2Cl2 / 24 h / 25 °C 2.1: NaBH4 / tetrahydrofuran / 36 h / 40 °C View Scheme
参考文献
Matsuo, Takashi; Imai, Chie; Yoshida, Takefumi; Saito, Takashi; Hayashi, Takashi; Hirota, Shun
Chemical Communications, 2012 , vol. 48, # 11 p. 1662 - 1664
反应条件
phosphate buffer; chymotrypsine T=25°C; hydrolysis, various substrates under different reaction conditions; Product distributionRate constant;
参考文献
Khurgin, Yu. I.; Perepechkina, T. L.
Russian Chemical Bulletin, 1993 , vol. 42, # 8 p. 1441 - 1442
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 8 p. 1503 - 1504