反应条件
1: 57 percent / NaH / dimethylformamide / 4.5 h / 0 - 20 °C 2: TfOH, NIS / diethyl ether; CH2Cl2 / 0.5 h / -15 °C 3: NaOMe / tetrahydrofuran; methanol / 19 h / Ambient temperature 4: NH2NH2 / 20 percent Pd(OH)2/C / methanol / 19 h / Heating 5: H2 / 20 percent Pd(OH)2/C / acetic acid; H2O / 22 h / 760 Torr / Ambient temperature View Scheme
参考文献
Greenberg, William A.; Priestley, E. Scott; Sears, Pamela S.; Alper, Phil B.; Rosenbohm, Christoph; Hendrix, Martin; Hung, Shang-Cheng; Wong, Chi-Huey
Journal of the American Chemical Society, 1999 , vol. 121, # 28 p. 6527 - 6541
