1,6-萘啶-2(1H)-酮合成路线 （共 14 条）
反应条件
in trichlorophosphate
参考文献
Wakabayashi, Toshiaki; Funahashi, Yasuhiro; Hata, Naoko; Semba, Taro; Yamamoto, Yuji; Haneda, Toru; Owa, Takashi; Tsuruoka, Akihiko; Kamata, Junichi; Okabe, Tadashi; Takahashi, Keiko; Nara, Kazumasa; Hamaoka, Shinichi; Ueda, Norihiro
Patent: US2004/18192 A1, 2004 ;
反应条件
1: 83 percent / fuming nitric acid, 20 percent oleum / 4 h / Heating
2: 44 percent / POCl3 / 8 h / Heating
3: 60 percent / NaOEt / ethanol / 3 h / Ambient temperature
View Scheme
参考文献
Wozniak, M.; Plas, H. C. van der; Tomula, M.; Veldhuizen, A. van
Recueil: Journal of the Royal Netherlands Chemical Society, 1983 , vol. 102, # 7-8 p. 359 - 363
反应条件
1: 83 percent / fuming nitric acid, 20 percent oleum / 4 h / Heating
2: 44 percent / POCl3 / 8 h / Heating
3: 75 percent / NH3(g) / ethanol / 4 h / 110 °C / autoclave
View Scheme
参考文献
Wozniak, M.; Plas, H. C. van der; Tomula, M.; Veldhuizen, A. van
Recueil: Journal of the Royal Netherlands Chemical Society, 1983 , vol. 102, # 7-8 p. 359 - 363
反应条件
1: 83 percent / fuming nitric acid, 20 percent oleum / 4 h / Heating
2: 44 percent / POCl3 / 8 h / Heating
3: 33 percent / KMnO4, liquid NH3 / 0.25 h
View Scheme
参考文献
Wozniak, M.; Plas, H. C. van der; Tomula, M.; Veldhuizen, A. van
Recueil: Journal of the Royal Netherlands Chemical Society, 1983 , vol. 102, # 7-8 p. 359 - 363
