2,5-二氯-1,6-萘啶合成路线 （共 2 条）
反应条件
1: trichlorophosphate / 24 h / 100 °C 2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 20 °C / |Cooling with ice 3: trichlorophosphate; triethylamine / dichloromethane / 2 h / 48 °C View Scheme
参考文献
CUREGENIX INC.; AN, Songzhu
Patent: WO2013/185353 A1, 2013 ;
反应条件
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 20 °C / |Cooling with ice 2: trichlorophosphate; triethylamine / dichloromethane / 2 h / 48 °C View Scheme
参考文献
CUREGENIX INC.; AN, Songzhu
Patent: WO2013/185353 A1, 2013 ;
