1,2-二(氯甲基)-4,5-二甲苯合成路线 (共 16 条)
反应条件
hydrogenchloride in water; 2-methyl cyclohexane T=60°C; 8 h;
参考文献
Hu; Liu; Lu; Ge; Zhang
Journal of the Iranian Chemical Society, 2011 , vol. 8, # 1 p. 131 - 141
反应条件
hydrogenchloride; 1-ethyl-3-methylimidazolium tetrafluoroborate T=70°C; 5 h;
参考文献
Wang, Yun; Xi, Yanli
Journal of the Chilean Chemical Society, 2013 , vol. 58, # 4 p. 2196 - 2199
反应条件
hydrogenchloride; zinc(II) chloride in acetic acid T=80 - 90°C; 36 h;
参考文献
Cagniant,P. et al.
Bulletin de la Societe Chimique de France, 1961 , p. 2225 - 2235
反应条件
hydrogenchloride; potassium permanganate in water 0.0833333 h; Photolysis;
参考文献
Zenkevich
Russian Journal of Organic Chemistry, 2001 , vol. 37, # 2 p. 270 - 280
反应条件
hydrogenchloride 2 h; Heating; Further byproducts. Title compound not separated from byproducts.;
参考文献
Zenkevich; Makarov
Russian Journal of General Chemistry, 2007 , vol. 77, # 4 p. 611 - 619
参考文献
v. Braun; Nelles
Chemische Berichte, 1934 , vol. 67, p. 1094,1096
Full Text Show Details
I.G. Farbenind.
Patent: DE509149 , 1927 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 17, p. 429
反应条件
tris(ammonia)chromium tricarbonyl in 1,4-dioxane T=101°C; 3.5 h; Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 123, # 1 p. 93 - 99
反应条件
dipotassium hydrogenphosphate; Potassium benzeneselenite in acetonitrile 3 h;
参考文献
Syper; Mlochowski
Synthesis, 1984 , vol. NO. 9, p. 747 - 752
反应条件
acetic acid Behandeln des oeligen Reaktionsprodukts mit Alkalilauge;
参考文献
v. Braun; Nelles
Chemische Berichte, 1934 , vol. 67, p. 1094,1096
反应条件
(i) iPrOH, H2O, (ii) aq. NH3; Multistep reaction;
参考文献
Shahak,I.; Bergmann,E.D.
Journal of the Chemical Society [Section] C: Organic, 1966 , p. 1005 - 1009