(S)-(+)-3-(苄氧基羰基)-5-氧代-4-噁唑啉丙酸合成路线 (共 21 条)
反应条件
toluene-4-sulfonic acid in toluene 1.67 h; Heating;
参考文献
Luesch, Hendrik; Hoffmann, Dietmar; Hevel, Joan M.; Becker, Julia E.; Golakoti, Trimurtulu; Moore, Richard E.
Journal of Organic Chemistry, 2003 , vol. 68, # 1 p. 83 - 91
反应条件
toluene-4-sulfonic acid in toluene Heating;
参考文献
Loffet, A.; Galeotti, N.; Jouin, P.; Castro, B.
Tetrahedron Letters, 1989 , vol. 30, # 49 p. 6859 - 6860
参考文献
Kubasch, Niels; Schmidt, Richard R.
European Journal of Organic Chemistry, 2002 , # 16 p. 2710 - 2726
反应条件
trifluoroacetic acid in dichloromethane T=20°C; Dealkylation;
参考文献
Synlett, , # 7 p. 1136 - 1138
反应条件
1: 98 percent / triethylamine / methanol / 3 h 2: 90 percent / toluenesulfonic acid / toluene / 3 h / Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 4 p. 1111 - 1118
反应条件
Yield given. Multistep reaction;
参考文献
Synthetic Communications, , vol. 18, # 14 p. 1707 - 1714
反应条件
boron trichloride in dichloromethane T=25°C; 0.333333 h;
参考文献
Allevi, Pietro; Cribiu, Riccardo; Anastasia, Mario
Tetrahedron Letters, 2004 , vol. 45, # 30 p. 5841 - 5843
反应条件
1: N-methylmorpholine / CH2Cl2 / 0.25 h / -10 °C 2: CH2Cl2; diethyl ether / 0 deg C, 30 min, -5 deg C, 4 h 3: 99 percent / PhCO2Ag, Et3N / tetrahydrofuran; H2O / 0.5 h / Ambient temperature View Scheme
参考文献
Pellicciari, Roberto; Natalini, Benedetto; Marinozzi, Maura
Synthetic Communications, 1988 , vol. 18, # 14 p. 1707 - 1714
反应条件
1.1: 100 percent / oxalyl chloride; DMF / CH2Cl2 / 0.5 h / 20 °C 2.1: 48 percent / D2; lutidine / 5percent Pd/BaSO4 / tetrahydrofuran / 2 h / 20 °C 3.1: 18 percent / (R)-Alpine borane / tetrahydrofuran / 10 h / 20 °C 4.1: 78 percent / hydrochloric acid / H2O / 2 h / 100 °C 5.1: NosE gene from Escherichia coli; β-NAD; ZnSO4 / glycine / H2O / 5 h / 42 °C / pH 10 5.2: NosF gene from Escherichia coli / H2O / 0.25 h / pH 10 View Scheme
参考文献
Luesch, Hendrik; Hoffmann, Dietmar; Hevel, Joan M.; Becker, Julia E.; Golakoti, Trimurtulu; Moore, Richard E.
Journal of Organic Chemistry, 2003 , vol. 68, # 1 p. 83 - 91
反应条件
1: 90 percent / sodium methoxide / methanol / 2 h / 0 °C 2: 60 percent / lead tetraacetate, cupric acetate monohydrate / benzene / 15 h / Heating View Scheme
参考文献
Hanessian, Stephen; Sahoo, Soumya P.
Tetrahedron Letters, 1984 , vol. 25, # 14 p. 1425 - 1428