反应条件
in tetrahydrofuran; hexane
(N2); addn. of a soln. of AlMe3 in hexane to a soln. of cobalt complex in THF at -15°C for 5 min, warming to room temp. over 0.5 h, stirring for 2.0 h; addn. of water, extn. with CH2Cl2, drying org. phase over MgSO4, evapn.,column chromy.;
参考文献
Pidaparthi, Ramakrishna R.; Welker, Mark E.; Day, Cynthia S.
Organometallics, 2006 , vol. 25, # 4 p. 974 - 981
