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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
23647-26-9
合成路线
（共 8 条）
23647-26-9
→
反应条件
66-71-7
1,10-菲罗啉
反应条件
sulfolane; triphenylphosphine T=151°C; Rate constant;
参考文献
Deady, Leslie W.
Australian Journal of Chemistry, 1981 , vol. 34, # 1 p. 163 - 170
23647-26-9
→
反应条件
29176-54-3
反应条件
1.1: potassium hexacyanoferrate(III); sodium hydroxide / water / 10 - 20 °C 2.1: phosphorus pentachloride; trichlorophosphate / Inert atmosphere; Cooling in ice; Reflux 2.2: Alkaline conditions 3.1: 20 - 120 °C / Inert atmosphere 4.1: potassium hexacyanoferrate(III); sodium hydroxide / water / 20 °C / Cooling with ice View Scheme
参考文献
B.R.A.H.M.S GmbH; HOSHINO, Mikio; YANO, Toshisada; YAMANAKA, Yasukazu
Patent: WO2012/124310 A1, 2012 ;
23647-26-9
→
反应条件
29176-55-4
2,9-二氯-1,10-菲罗啉
反应条件
1.1: potassium hexacyanoferrate(III); sodium hydroxide / water / 10 - 20 °C 2.1: phosphorus pentachloride; trichlorophosphate / Inert atmosphere; Cooling in ice; Reflux 2.2: Alkaline conditions 3.1: 20 - 120 °C / Inert atmosphere 4.1: potassium hexacyanoferrate(III); sodium hydroxide / water / 20 °C / Cooling with ice 5.1: phosphorus pentachloride; trichlorophosphate / Inert atmosphere; cooling with ice; Reflux 5.2: Alkaline conditions View Scheme
参考文献
B.R.A.H.M.S GmbH; HOSHINO, Mikio; YANO, Toshisada; YAMANAKA, Yasukazu
Patent: WO2012/124310 A1, 2012 ;
23647-26-9
→
反应条件
7089-68-1
2-氯-1,10-邻二氮杂菲
反应条件
1.1: potassium hexacyanoferrate(III); sodium hydroxide / water / 10 - 20 °C 2.1: phosphorus pentachloride; trichlorophosphate / Inert atmosphere; Cooling in ice; Reflux 2.2: Alkaline conditions View Scheme
参考文献
B.R.A.H.M.S GmbH; HOSHINO, Mikio; YANO, Toshisada; YAMANAKA, Yasukazu
Patent: WO2012/124310 A1, 2012 ;
23647-26-9
→
反应条件
31535-89-4
1-甲基-1,10-菲罗啉-2(1H)-酮
反应条件
K3Fe(CN)6; sodium hydroxide in water T=45 - 60°C; 18 h;
参考文献
Boettger, Matthias; Wiegmann, Bjoern; Schaumburg, Steffen; Jones, Peter G.; Kowalsky, Wolfgang; Johannes, Hans-Hermann
Beilstein Journal of Organic Chemistry, 2012 , vol. 8, p. 1037 - 1047
23647-26-9
→
反应条件
22426-14-8
2-溴-1,10-菲罗啉
反应条件
1.1: potassium hexacyanoferrate(III); sodium hydroxide / water / 10 - 20 °C 2.1: phosphorus pentabromide; phosphorus oxytribromide / 20 - 80 °C / Inert atmosphere 2.2: Alkaline conditions View Scheme
参考文献
B.R.A.H.M.S GmbH; HOSHINO, Mikio; YANO, Toshisada; YAMANAKA, Yasukazu
Patent: WO2012/124310 A1, 2012 ;
23647-26-9
→
反应条件
39069-01-7
反应条件
1.1: potassium hexacyanoferrate(III); sodium hydroxide / water / 10 - 20 °C 2.1: phosphorus pentabromide; phosphorus oxytribromide / 20 - 80 °C / Inert atmosphere 2.2: Alkaline conditions 3.1: 120 °C / Inert atmosphere; cooling with ice 4.1: potassium hexacyanoferrate(III); sodium hydroxide / water / 4 - 20 °C View Scheme
参考文献
B.R.A.H.M.S GmbH; HOSHINO, Mikio; YANO, Toshisada; YAMANAKA, Yasukazu
Patent: WO2012/124310 A1, 2012 ;
23647-26-9
→
反应条件
39069-02-8
2,9-二溴-1,10-菲罗啉
反应条件
1.1: potassium hexacyanoferrate(III); sodium hydroxide / water / 10 - 20 °C 2.1: phosphorus pentabromide; phosphorus oxytribromide / 20 - 80 °C / Inert atmosphere 2.2: Alkaline conditions 3.1: 120 °C / Inert atmosphere; cooling with ice 4.1: potassium hexacyanoferrate(III); sodium hydroxide / water / 4 - 20 °C 5.1: phosphorus pentabromide; phosphorus oxytribromide / 75 °C / Inert atmosphere; cooling with ice 5.2: Alkaline conditions View Scheme
参考文献
B.R.A.H.M.S GmbH; HOSHINO, Mikio; YANO, Toshisada; YAMANAKA, Yasukazu
Patent: WO2012/124310 A1, 2012 ;
