反应条件
1: 1.) 2.6 M n-BuLi, 2.) fluoropicoline / 1.) diethyl ether, -65 deg C, 1 h, 2.) diethyl ether, -40 deg C to -30 deg C, 30 min
2: 60 percent / potassium permanganate / H2O / 1.75 h / Heating
3: 85 percent / polyphosphoric acid / 4.5 h / 210 °C
4: 80 percent / hydrazine monohydrate / bis-(2-hydroxy-ethyl) ether / 4 h / 180 °C
View Scheme
参考文献
DuPriest, Mark T.; Schmidt, Charles L.; Kuzmich, Daniel; Williams, Stanly B
Journal of Organic Chemistry, 1986 , vol. 51, # 11 p. 2021 - 2023
