magnesium in diethyl ether
(N2); a mixture of (CH3)3SnCH2I and Mg in ether refluxed for 1 h; a soln. of (CH3)3GeBr added dropwise over a period of 45 min; refluxed for 1 h and stirred overnight; treated with saturated NH4Cl; distd.;
参考文献
Hawker, Darryl W.; Wells, Peter R.
Organometallics, 1985 , vol. 4, p. 821 - 825
magnesium in diethyl ether
(N2); a mixture of (CH3)3SnCH2I and Mg in ether refluxed for 1 h; a soln. of (CH3)3GeBr added dropwise over a period of 45 min; refluxed for 1 h and stirred overnight; treated with saturated NH4Cl; distd.;
参考文献
Hawker, Darryl W.; Wells, Peter R.
Organometallics, 1985 , vol. 4, p. 821 - 825
