4-甲基-n-(2-甲基丙基)苯磺酰胺合成路线 (共 8 条)
反应条件
triethylsilane; boron trifluoride diethyl etherate in benzene T=5°C;
参考文献
Alexander, Michael D.; Anderson, Robert E.; Sisko, Joseph; Weinreb, Steven M.
Journal of Organic Chemistry, 1990 , vol. 55, # 8 p. 2563 - 2564
反应条件
Raney-Ni in ethanol T=20°C; 2 h;
参考文献
Ruano, Jose Luis Garca; Fernandez-Salas, Jose A.; Maestro, M. Carmen; Parra, Alejandro
Synthetic Communications, 2013 , vol. 43, # 2 p. 198 - 207,10
反应条件
copper(ll) bromide in dimethyl sulfoxide T=100°C; 24 h; Inert atmosphere; chemoselective reaction;
参考文献
Tang, Xiaodong; Huang, Liangbin; Qi, Chaorong; Wu, Xia; Wu, Wanqing; Jiang, Huanfeng
Chemical Communications, 2013 , vol. 49, # 54 p. 6102 - 6104
参考文献
White, Emil H.; Lewis, Charles P.; Ribi, Max A.; Ryan, Thomas J.
Journal of Organic Chemistry, 1981 , vol. 46, # 3 p. 552 - 558
反应条件
titanium tetrachloride in tetrachloroethane, 1,1,2,2- T=120°C; 48 h; sealed tube;
参考文献
Chen, Jiayan; Dang, Ling; Li, Qiang; Ye, Yong; Fu, Shaomin; Zeng, Wei
Synlett, 2012 , # 4 p. 595 - 600
反应条件
ethyldimethylsilane; (Ace)Ru3(CO)7 in dichloromethane T=20°C; 6 h; Inert atmosphere;
参考文献
Nishikata, Takashi; Nagashima, Hideo
Angewandte Chemie - International Edition, 2012 , vol. 51, # 22 p. 5363 - 5366
反应条件
2: Raney-Ni / ethanol / 2 h / 20 °C View Scheme
参考文献
Ruano, Jose Luis Garca; Fernandez-Salas, Jose A.; Maestro, M. Carmen; Parra, Alejandro
Synthetic Communications, 2013 , vol. 43, # 2 p. 198 - 207,10
反应条件
sodium carbonate in chlorobenzene T=130°C; 20 h; Product distributionMechanism;
参考文献
White, Emil H.; Lewis, Charles P.; Ribi, Max A.; Ryan, Thomas J.
Journal of Organic Chemistry, 1981 , vol. 46, # 3 p. 552 - 558