3-(6-甲氧基-2-萘基)苯甲醛合成路线 （共 5 条）
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in toluene Suzuki coupling; 16 h; Heating;
参考文献
Pinto-Bazurco Mendieta, Mariano A.E.; Negri, Matthias; Jagusch, Carsten; Hille, Ulrike E.; Mueller-Vieira, Ursula; Schmidt, Dirk; Hansen, Klaus; Hartmann, Rolf W.
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 1 p. 267 - 273
反应条件
1: 1) Mg, I2 / 2) Pd(PPh3)4 / 1) THF, reflux, 2 h, 2) THF, reflux, 2 h 2: aq. HCl / tetrahydrofuran / 10 h / Ambient temperature View Scheme
参考文献
Zhuang, Yan; Hartmann, Rolf W.
Archiv der Pharmazie, 1999 , vol. 332, # 1 p. 25 - 30
反应条件
1: 68 percent / TsOH*H2O / toluene / 104 h / Heating 2: 1) Mg, I2 / 2) Pd(PPh3)4 / 1) THF, reflux, 2 h, 2) THF, reflux, 2 h 3: aq. HCl / tetrahydrofuran / 10 h / Ambient temperature View Scheme
参考文献
Zhuang, Yan; Hartmann, Rolf W.
Archiv der Pharmazie, 1999 , vol. 332, # 1 p. 25 - 30
反应条件
1: 1) Mg, I2 / 2) Pd(PPh3)4 / 1) THF, reflux, 2 h, 2) THF, reflux, 2 h 2: aq. HCl / tetrahydrofuran / 10 h / Ambient temperature View Scheme
参考文献
Zhuang, Yan; Hartmann, Rolf W.
Archiv der Pharmazie, 1999 , vol. 332, # 1 p. 25 - 30
反应条件
hydrogenchloride in tetrahydrofuran 10 h; Ambient temperature; Yield given;
参考文献
Zhuang, Yan; Hartmann, Rolf W.
Archiv der Pharmazie, 1999 , vol. 332, # 1 p. 25 - 30
