3,4-(亚甲二氧)肉桂酸合成路线 （共 62 条）
反应条件
tert.-butylnitrite; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical in acetonitrile T=50°C; 6 h; stereoselective reaction;
参考文献
Manna, Srimanta; Jana, Sandipan; Saboo, Tapish; Maji, Arun; Maiti, Debabrata
Chemical Communications, 2013 , vol. 49, # 46 p. 5286 - 5288
反应条件
oxalyl dichloride in dichloromethane T=25°C;
参考文献
Lampe et al.
Roczniki Chemii, 1929 , vol. 9, p. 458
反应条件
pyridine; thionyl chloride in N,N-dimethyl-formamide 1.) reflux, 4 h, 2.) 140-150 deg C, 1 h; Yields of byproduct given;
参考文献
Gakhar, H. K.; Kaur, R.; Gupta, S. B.
Monatshefte fuer Chemie, 1995 , vol. 126, # 11 p. 1253 - 1256
反应条件
nitric acid β-<6-nitro-3.4-methylenedioxy-phenyl>-acrylic acid;
参考文献
Perkin,F. M.
Journal of the Chemical Society, 1891 , vol. 59, p. 152
反应条件
1: 10 palladium on activated charcoal; hydrogen 2: oxalyl dichloride / dichloromethane 3: tin(IV) chloride View Scheme
参考文献
Barltrop
Journal of the Chemical Society, 1946 , p. 958,962
反应条件
1: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in 1,4-dioxane; water 2: With sodium hydroxide Heating;
参考文献
Petzer, Jacobus P.; Steyn, Salome; Castagnoli, Kay P.; Chen, Jiang-Fan; Schwarzschild, Michael A.; Van Der Schyf, Cornelis J.; Castagnoli, Neal
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 7 p. 1299 - 1310
反应条件
1: LAH / tetrahydrofuran / 20 °C 2: 71 percent / TPAP; 4 Angstroem molecular sieves / CH2Cl2 View Scheme
参考文献
Browder; Marmsaeter; West
Organic letters, 2001 , vol. 3, # 19 p. 3033 - 3035
反应条件
tert.-butylnitrite; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical in acetonitrile T=50°C; 6 h; stereoselective reaction;
参考文献
Manna, Srimanta; Jana, Sandipan; Saboo, Tapish; Maji, Arun; Maiti, Debabrata
Chemical Communications, 2013 , vol. 49, # 46 p. 5286 - 5288
参考文献
Posner
Justus Liebigs Annalen der Chemie, 1912 , vol. 389, p. 36,111
反应条件
sodium hydroxide; nickel monoaluminide
参考文献
Salway
Journal of the Chemical Society, 1910 , vol. 97, p. 2417
