1: 24.3 g / potassium fluoride / dimethylformamide / 4 h / 120 - 130 °C 2: 1.0 g / phosphoryl chloride / 1.) from -5 deg C to RT, 2.) 100 deg C, 2 h View Scheme

trichlorophosphate 1.) from -5 deg C to RT, 2.) 100 deg C, 2 h;