4-溴-2,6-二甲基苯酚合成路线 (共 34 条)
反应条件
in 1,4-dioxane; diethyl ether MechanismProduct distribution;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 23 p. 1617 - 1619
反应条件
oxygen; copper dichloride in water; N,N-dimethyl-formamide T=60°C; 16 h;
参考文献
THE REGENTS OF THE UNIVERSITY OF CALIFORNIA
Patent: US2007/203080 A1, 2007 ;
Location in patent: Page/Page column 33 ;
反应条件
nitric acid in acetic acid T=20°C; 0.166667 h; Further byproducts given;
参考文献
Hartshorn, Michael P.; Readman, Jennifer M.; Robinson, Ward T.; Vaughan, John; Whyte, Andrew R.
Australian Journal of Chemistry, 1985 , vol. 38, # 11 p. 1693 - 1704
反应条件
1: 1) t-BuLi / 1) THF, pentane, -78 deg C, 2) 0 deg C, 25 min 2: 1) Me3SiBr, 2) LiAlH4 / 1) THF, 10 min, 2) 0 deg C, 30 min View Scheme
参考文献
Journal of Organic Chemistry, , vol. 57, # 22 p. 5937 - 5947
反应条件
sodium hydroxide in water; isopropyl alcohol T=60°C; 15 h;
参考文献
WO2008/29306 A2, ;
Page/Page column 30 ;
WO 2008/029306 A2
反应条件
sodium hydroxide in water; isopropyl alcohol T=60°C; 15 h;
参考文献
WO2008/35239 A1, ;
Page/Page column 28-29 ;
反应条件
sodium hydroxide in water; isopropyl alcohol T=65°C; 15 h;
参考文献
Journal of Medicinal Chemistry, , vol. 56, # 23 p. 9737 - 9755
反应条件
potassium carbonate in acetone
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , # 9 p. 1824 - 1834
反应条件
potassium hydroxide in 1,4-dioxane 96 h; Heating;
参考文献
Vajda; Kaspar; Hamplova; Vanek; Fodor-Csorba; Bata
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 2001 , vol. 351, p. 279 - 286
反应条件
in water; N,N-dimethyl-formamide
参考文献
Aspnes, Gary E.; Chiang, Yuan-Ching P.
Patent: US2002/6946 A1, 2002 ;
US 20020006946 A1