5-(2-氯苯基)-[1,3,4]噁二唑-2-硫醇合成路线 （共 10 条）
反应条件
1: With potassium hydroxide in ethanol 6 h; Reflux; 2: With hydrogenchloride; water
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 20, # 12 p. 3755 - 3759
反应条件
in N,N-dimethyl-formamide 0.00833333 h; Irradiation;
参考文献
Joshi, Sachin; Karnik
Synthetic Communications, 2002 , vol. 32, # 1 p. 111 - 114
反应条件
1: 87 percent / hydrazine hydrate / ethanol 2: 86 percent / dimethylformamide View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 16 p. 4842 - 4850
反应条件
1: sulfuric acid / |Reflux 2: hydrazine hydrate / methanol / |Reflux 3: potassium hydroxide / methanol / |Reflux View Scheme
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 187, # 11 p. 1401 - 1408
反应条件
in N,N-dimethyl-formamide
参考文献
Macaev, Fliur; Rusu, Ghenadie; Pogrebnoi, Serghei; Gudima, Alexandru; Stingaci, Eugenia; Vlad, Ludmila; Shvets, Nathaly; Kandemirli, Fatma; Dimoglo, Anatholy; Reynolds, Robert
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 16 p. 4842 - 4850
反应条件
1: hydrazine hydrate / ethanol / |Reflux 2: potassium hydroxide / ethanol / |Reflux View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 21, # 8 p. 2286 - 2297
反应条件
1: triethylamine / dichloromethane / 0 °C 2: hydrazine hydrate / methanol / 5 h / |Reflux 3: potassium hydroxide / methanol / 20 °C / |Reflux 4: hydrogenchloride / water / 0 - 5 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 24, # 1 p. 192 - 194
反应条件
1: potassium hydroxide / methanol / 20 °C / |Reflux 2: hydrogenchloride / water / 0 - 5 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 24, # 1 p. 192 - 194
反应条件
sodium hydroxide; ethanol 2.) EtOH, reflux, 5 h; Yield given. Multistep reaction;
参考文献
Yadav, Lal Dhar S.; Pal, Daya R.
Journal of Chemical Research - Part S, 1997 , # 3 p. 90 - 91
反应条件
hydrazine hydrate 3 h; Heating;
参考文献
Joshi; Karnik
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 4 p. 1057 - 1059
