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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
23783-80-4
合成路线
（共 13 条）
123-31-9
对苯二酚
→
反应条件
23783-80-4
反应条件
oxygen; acetic acid; bis(1,3-propanediaminato)copper(II) chloride in ethanol 3 h; Heating;
参考文献
Paraskevas, Spyridon M.; Konstantinidis, Demetrios; Vassilara, Georgia
Synthesis, 1988 , # 11 p. 897 - 899
4555-64-0
→
反应条件
23783-80-4
反应条件
ammonium cerium(IV) nitrate in water; acetonitrile 0.5 h; cooling;
参考文献
Bovicelli, Paolo; Antonioletti, Roberto; Onori, Antonella; Delogu, Giovanna; Fabbri, Davide; Dettori, Maria Antonietta
Tetrahedron, 2006 , vol. 62, # 4 p. 635 - 639
1806-29-7
2,2'-二羟基联苯
→
反应条件
23783-80-4
+
25483-66-3
反应条件
Fremy’s salt in water; acetone T=20°C; 2 h;
参考文献
Bouaziz, Zouhair; Gherardi, Arnaud; Regnier, Francois; Sarciron, Marie-Elizabeth; Bertheau, Xavier; Fenet, Bernard; Walchshofer, Nadia; Fillion, Houda
European Journal of Organic Chemistry, 2002 , # 11 p. 1834 - 1838
1806-29-7
2,2'-二羟基联苯
→
反应条件
23783-80-4
反应条件
perchloric acid; lead dioxide T=0°C; 0.5 h;
参考文献
Ryu, Chung-Kyu; Lee, Seung-Yon; Kim, Na Young; Hong, Jung An; Yoon, Joo Hee; Kim, Aram
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 1 p. 427 - 430
875714-47-9
→
反应条件
23783-80-4
反应条件
ammonium cerium(IV) nitrate in water; acetonitrile 0.666667 h; cooling;
参考文献
Bovicelli, Paolo; Antonioletti, Roberto; Onori, Antonella; Delogu, Giovanna; Fabbri, Davide; Dettori, Maria Antonietta
Tetrahedron, 2006 , vol. 62, # 4 p. 635 - 639
875714-46-8
→
反应条件
23783-80-4
反应条件
1: 75 percent / sodium methylate; CuBr / dimethylformamide; H2O / 2 h / Heating 2: 80 percent / cerium(IV) ammonium nitrate / acetonitrile; H2O / 0.67 h / cooling View Scheme
参考文献
Bovicelli, Paolo; Antonioletti, Roberto; Onori, Antonella; Delogu, Giovanna; Fabbri, Davide; Dettori, Maria Antonietta
Tetrahedron, 2006 , vol. 62, # 4 p. 635 - 639
220-11-1
→
反应条件
23783-80-4
反应条件
1: 90 percent / NaBr; oxone / acetone; H2O 2: 75 percent / sodium methylate; CuBr / dimethylformamide; H2O / 2 h / Heating 3: 80 percent / cerium(IV) ammonium nitrate / acetonitrile; H2O / 0.67 h / cooling View Scheme
参考文献
Bovicelli, Paolo; Antonioletti, Roberto; Onori, Antonella; Delogu, Giovanna; Fabbri, Davide; Dettori, Maria Antonietta
Tetrahedron, 2006 , vol. 62, # 4 p. 635 - 639
4877-93-4
2,2’-二甲氧基联苯
→
反应条件
23783-80-4
反应条件
1: 80 percent / H2SO4; dimethyldioxirane; NaBr / acetone 2: 60 percent / sodium methylate; CuBr / dimethylformamide; H2O / 2 h / Heating 3: 90 percent / cerium ammonium nitrate / acetonitrile; H2O / 0.5 h / cooling View Scheme
参考文献
Bovicelli, Paolo; Antonioletti, Roberto; Onori, Antonella; Delogu, Giovanna; Fabbri, Davide; Dettori, Maria Antonietta
Tetrahedron, 2006 , vol. 62, # 4 p. 635 - 639
100542-54-9
→
反应条件
23783-80-4
反应条件
1: 60 percent / sodium methylate; CuBr / dimethylformamide; H2O / 2 h / Heating 2: 90 percent / cerium ammonium nitrate / acetonitrile; H2O / 0.5 h / cooling View Scheme
参考文献
Bovicelli, Paolo; Antonioletti, Roberto; Onori, Antonella; Delogu, Giovanna; Fabbri, Davide; Dettori, Maria Antonietta
Tetrahedron, 2006 , vol. 62, # 4 p. 635 - 639
4371-32-8
[1,1'-联苯基]-2,2',5,5'-四醇
→
反应条件
23783-80-4
反应条件
water; iron(III) chloride
参考文献
Teuber; Rau
Chemische Berichte, 1953 , vol. 86, p. 1036,1044
Full Text Show Details
Erdtman et al.
Acta Chemica Scandinavica (1947-1973), 1954 , vol. 8, p. 1442,1446
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