反应条件
1: 100 percent / LDA; DMPU / tetrahydrofuran / -78 °C 2: 98 percent / LiAlH4 / diethyl ether / 20 °C 3: DMSO; (COCl)2; Et3N / CH2Cl2 / -78 °C 4: benzene / 60 °C 5: 89 percent / H2 / Pd/C / ethyl acetate / 20 °C 6: 92 percent / tetrahydrofuran / 0 °C 7: 91 percent / mCPBA; NaHCO3 / CH2Cl2 / 20 °C 8: 100 percent / LTMP; Et2AlCl / toluene / 0 °C 9: 96 percent / OsO4; NMO / tetrahydrofuran; H2O / 20 °C 10: NaIO4 / tetrahydrofuran; H2O / 20 °C 11: dimethylsulfoxide / 40 °C 12: LiAlH4 / tetrahydrofuran 13: DMSO; (COCl)2; Et3N / CH2Cl2 / -78 °C 14: dimethylsulfoxide / 40 °C 15: 85 percent / Ph2PLi / tetrahydrofuran / 50 °C View Scheme
参考文献
Ohira, Susumu; Kuboki, Atsuhito; Hasegawa, Taisuke; Kikuchi, Takato; Kutsukake, Tatsuhiko; Nomura, Maki
Tetrahedron Letters, 2002 , vol. 43, # 26 p. 4641 - 4644
