您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
5-羟基-6-甲氧基吲哚
合成路线
（共 8 条）
98258-77-6
→
反应条件
2380-83-8
5-羟基-6-甲氧基吲哚
反应条件
hydrogen; palladium on activated charcoal in methanol P=775.7 Torr; 2 h;
参考文献
Rogers, C. Bradford; Blum, Charles A.; Murphy, Bryan P.
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 941 - 943
58749-47-6
5-羟基-4-甲氧基-2-硝基苯甲醛
→
反应条件
2380-83-8
5-羟基-6-甲氧基吲哚
反应条件
1: 98 percent / 4-(dimethylamino)pyridine / 1 h 2: KF, 18-crown-8 / propan-2-ol / 5 h 3: acetic anhydride, sodium acetate / overnight 4: 94 percent / K2CO3 / ethanol / Ambient temperature 5: 43 percent / H2 / 10percent Pd/C / methanol / 2 h / 775.7 Torr View Scheme
参考文献
Rogers, C. Bradford; Blum, Charles A.; Murphy, Bryan P.
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 941 - 943
58662-50-3
5-苄氧基-4-甲氧基-2-硝基苯甲醛
→
反应条件
2380-83-8
5-羟基-6-甲氧基吲哚
反应条件
1: CF3COOH / 60 °C 2: 98 percent / 4-(dimethylamino)pyridine / 1 h 3: KF, 18-crown-8 / propan-2-ol / 5 h 4: acetic anhydride, sodium acetate / overnight 5: 94 percent / K2CO3 / ethanol / Ambient temperature 6: 43 percent / H2 / 10percent Pd/C / methanol / 2 h / 775.7 Torr View Scheme
参考文献
Rogers, C. Bradford; Blum, Charles A.; Murphy, Bryan P.
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 941 - 943
112919-68-3
→
反应条件
2380-83-8
5-羟基-6-甲氧基吲哚
反应条件
1: 94 percent / K2CO3 / ethanol / Ambient temperature 2: 43 percent / H2 / 10percent Pd/C / methanol / 2 h / 775.7 Torr View Scheme
参考文献
Rogers, C. Bradford; Blum, Charles A.; Murphy, Bryan P.
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 941 - 943
112919-66-1
→
反应条件
2380-83-8
5-羟基-6-甲氧基吲哚
反应条件
1: KF, 18-crown-8 / propan-2-ol / 5 h 2: acetic anhydride, sodium acetate / overnight 3: 94 percent / K2CO3 / ethanol / Ambient temperature 4: 43 percent / H2 / 10percent Pd/C / methanol / 2 h / 775.7 Torr View Scheme
参考文献
Rogers, C. Bradford; Blum, Charles A.; Murphy, Bryan P.
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 941 - 943
6346-05-0
3-苄氧基-4-甲氧基苯甲醛
→
反应条件
2380-83-8
5-羟基-6-甲氧基吲哚
反应条件
1: fumic HNO3 / 1,2-dichloro-ethane / 3 h / -15 °C 2: CF3COOH / 60 °C 3: 98 percent / 4-(dimethylamino)pyridine / 1 h 4: KF, 18-crown-8 / propan-2-ol / 5 h 5: acetic anhydride, sodium acetate / overnight 6: 94 percent / K2CO3 / ethanol / Ambient temperature 7: 43 percent / H2 / 10percent Pd/C / methanol / 2 h / 775.7 Torr View Scheme
参考文献
Rogers, C. Bradford; Blum, Charles A.; Murphy, Bryan P.
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 941 - 943
141939-51-7
→
反应条件
2380-83-8
5-羟基-6-甲氧基吲哚
反应条件
1: 90 percent / p-toluenesulfonic acid / acetonitrile / 3 h / Ambient temperature 2: 10percent Pd/C / benzene / 3 h / Heating View Scheme
参考文献
Kita, Yasuyuki; Tohma, Hirofumi; Inagaki, Masanao; Hatanaka, Kenji
Heterocycles, 1992 , vol. 33, # 2 p. 503 - 506
141939-58-4
→
反应条件
2380-83-8
5-羟基-6-甲氧基吲哚
反应条件
1: phenyliodine bis(trifluoroacetate) (PIFA) / acetonitrile; H2O / 0.17 h / Ambient temperature 2: 90 percent / p-toluenesulfonic acid / acetonitrile / 3 h / Ambient temperature 3: 10percent Pd/C / benzene / 3 h / Heating View Scheme
参考文献
Kita, Yasuyuki; Tohma, Hirofumi; Inagaki, Masanao; Hatanaka, Kenji
Heterocycles, 1992 , vol. 33, # 2 p. 503 - 506
