2,2-二甲基丙醛氨基甲酰腙合成路线 (共 5 条)
参考文献
Lengyel, Istvan; Cesare, Victor; Taldone, Tony
Tetrahedron, 2004 , vol. 60, # 5 p. 1107 - 1124
反应条件
1: 1,3-ditert-butyl-2-aziridinone With trifluoroacetic acid in benzene T=20°C; 72 h; 2: semicarbazide-hydrochloride With sodium acetate T=20°C; 48 h; Further stages.;
参考文献
Lengyel, Istvan; Cesare, Victor; Taldone, Tony
Tetrahedron, 2004 , vol. 60, # 5 p. 1107 - 1124
反应条件
1: 1-(1-adamantyl)-3-tert-butylaziridinone With trifluoroacetic acid in benzene T=20°C; 66 h; 2: semicarbazide-hydrochloride With sodium acetate T=20°C; 7.5 h; Further stages.;
参考文献
Lengyel, Istvan; Cesare, Victor; Taldone, Tony
Tetrahedron, 2004 , vol. 60, # 5 p. 1107 - 1124
反应条件
sodium acetate in decane T=174°C; 1 h; distillation into receiving flask;
参考文献
Lengyel; Cesare; Taldone; Uliss
Synthetic Communications, 2001 , vol. 31, # 23 p. 3671 - 3683
反应条件
sulfuric acid T=130°C;
参考文献
Danilow; Venus-Danilowa
Chemische Berichte, 1926 , vol. 59, p. 381
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1925 , vol. 57, p. 352