2-甲基-1H-苯并(去)异喹啉-1,3(2H)-二酮合成路线 （共 19 条）
反应条件
1: With [2,2']bipyridinyl; nickel dichloride; zinc in N,N-dimethyl-formamide
T=70°C; 6 h;
2: With hydrogenchloride in N,N-dimethyl-formamide
T=30 - 40°C; 0.5 h; Title compound not separated from byproducts;
参考文献
Adonin; Ryabinin; Starichenko
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 6 p. 861 - 865
反应条件
in methanol
T=130°C; sealed tube; other temperature; Rate constantKineticsThermodynamic data;
参考文献
Plakidin, V. L.; Vostrova, V. N.
Journal of Organic Chemistry USSR (English Translation), 1983 , p. 2273 - 2281
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 12 p. 2591 - 2600
反应条件
in methanol
T=130°C; sealed tube;; Rate constant;
参考文献
Plakidin, V. L.; Vostrova, V. N.
Journal of Organic Chemistry USSR (English Translation), 1983 , p. 2273 - 2281
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 12 p. 2591 - 2600
反应条件
in methanol
T=130°C; 18 h; sealed tube;
参考文献
Plakidin, V. L.; Vostrova, V. N.
Journal of Organic Chemistry USSR (English Translation), 1983 , p. 2273 - 2281
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 12 p. 2591 - 2600
反应条件
in methanol
T=130°C; 18 h; sealed tube;
参考文献
Plakidin, V. L.; Vostrova, V. N.
Journal of Organic Chemistry USSR (English Translation), 1983 , p. 2273 - 2281
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 12 p. 2591 - 2600
参考文献
Jaubert
Chemische Berichte, 1895 , vol. 28, p. 360
Gazzetta Chimica Italiana, 1895 , vol. 25 I, p. 248
参考文献
Selden Co.
Patent: US1919889 , 1929 ;
反应条件
1.) H2O, 2.) nitrobenzene, reflux; Multistep reaction;
参考文献
Brun, Anne M.; Harriman, Anthony; Tsuboi, Yasuyuki; Okada, Tadashi; Mataga, Noboru
Journal of the Chemical Society, Faraday Transactions, 1995 , vol. 91, # 22 p. 4047 - 4058
参考文献
Bradley; Pexton
Journal of the Chemical Society, 1954 , p. 4436,4437
