腺苷酰基-(3,’5’)-胞苷合成路线 （共 20 条）
反应条件
1: 1.) 2,4,6-collidine / 1.) THF, -78 deg C, 10 min, 2.) THF, -78 deg C, 15 min; 20 deg C, 30 min 2: 70 percent / 2 percent benzenesulfonic acid / CHCl3; methanol / 2 h / Ambient temperature 3: 1.) t-butylamine, 2.) methanolic ammonia, 3.) TBAF View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 58, p. 2686 - 2693
反应条件
1: 1.) 2,4,6-collidine / 1.) THF, -78 deg C, 10 min, 2.) THF, -78 deg C, 15 min; 20 deg C, 30 min 2: 70 percent / 2 percent benzenesulfonic acid / CHCl3; methanol / 2 h / Ambient temperature 3: 1.) t-butylamine, 2.) methanolic ammonia, 3.) TBAF View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 58, p. 2686 - 2693
反应条件
1: 90 percent / 2 percent benzenesulfonic acid / CHCl3; methanol / 2 h / Ambient temperature 2: 1.) Zn/Cu couple, 2.) methanolic ammonia, 3.) TBAF View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 58, p. 2686 - 2693
反应条件
1: 85 percent / 2 percent benzenesulfonic acid / CHCl3; methanol / 2 h / Ambient temperature View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 58, p. 2686 - 2693
反应条件
1: 70 percent / 2 percent benzenesulfonic acid / CHCl3; methanol / 2 h / Ambient temperature 2: 1.) t-butylamine, 2.) methanolic ammonia, 3.) TBAF View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 58, p. 2686 - 2693
反应条件
ribonuclease-I Ribonuclease-I aus Rinder-Pancreas;
参考文献
Biochemical Journal, , vol. 60, p. 8,11
反应条件
hydrogenchloride; ammonium hydroxide; zinc(II) chloride Yield given. Multistep reaction;
参考文献
Chemistry Letters, , p. 197 - 200
反应条件
tetrabutyl ammonium fluoride; ammonia; copper; zinc Yield given. Multistep reaction;
参考文献
Canadian Journal of Chemistry, , vol. 58, p. 2686 - 2693
反应条件
1,4-dioxane; tributyl-amine; phenylphosphorochloridate Erwaermen des Reaktionsprodukts mit wss.NH3;
参考文献
Journal of the Chemical Society, , p. 3655,3664,3666
Biochemical Preparations, , vol. 10, p. 131
反应条件
(Zn(2+))3(1,3,5-tris[(1,5,9-triazacyclododecan-3-yl)oxymethyl]benzene)(6+) in water T=35°C; pH=7.5; aq. buffer; Kinetics; regioselective reaction;
参考文献
Organic and Biomolecular Chemistry, , vol. 7, # 13 p. 2780 - 2787
