4-氨基-1-苯基-1,2,5,6-四氢-3-膦甲腈合成路线 (共 6 条)
反应条件
hydrogenchloride 10 h; Heating;
参考文献
Gallagher,M.J.; Mann,F.G.
Journal of the Chemical Society, 1962 , p. 5110 - 5120
反应条件
1: aq. HCl / Heating 2: LiAlH4 / tetrahydrofuran / Heating View Scheme
参考文献
Mathey,F.; Muller,G.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1969 , vol. 269, p. 158 - 161
反应条件
sodium t-butanolate in toluene
参考文献
Welcher,R.P. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 4437 - 4438
反应条件
1: aq. HCl
2: (i) AcOH, H2O, (ii) HCl, EtOH
View Scheme
参考文献
Gallagher,M.J.; Mann,F.G.
Journal of the Chemical Society, 1962 , p. 5110 - 5120
反应条件
1: (i) Ac2O, (ii) aq. NH3, EtOH
2: D(-)-mandelic acid / ethanol / Heating
View Scheme
参考文献
Snider; Berlin
The Journal of organic chemistry, 1973 , vol. 38, # 9 p. 1657 - 1662
反应条件
(i) Ac2O, (ii) NaSH, EtOH; Multistep reaction;
参考文献
Snider; Berlin
The Journal of organic chemistry, 1973 , vol. 38, # 9 p. 1657 - 1662