2-甲基-3-苯基喹唑啉-4(3H)-酮合成路线 （共 32 条）
反应条件
in tetrahydrofuran
T=-78 - 20°C; 3 h;
参考文献
Nakano, Hayato; Kutsumura, Noriki; Saito, Takao
Synthesis (Germany), 2012 , vol. 44, # 20 p. 3179 - 3184
反应条件
in tetrahydrofuran
T=-78°C; 1 h;
参考文献
Nakano, Hayato; Kutsumura, Noriki; Saito, Takao
Synthesis (Germany), 2012 , vol. 44, # 20 p. 3179 - 3184
反应条件
PPh3.Br2 in dichloromethane
3 h; Heating;
参考文献
Mazurkiewicz, Roman
Monatshefte fuer Chemie, 1989 , vol. 120, p. 973 - 980
反应条件
1: copper(l) iodide; caesium carbonate; (2S,4R)-2-carboxy-4-hydroxypyrrolidine / N,N-dimethyl-formamide / 24 h / 80 °C / Inert atmosphere
2: 1,1,1,3,3,3-hexamethyl-disilazane; zinc(II) chloride / N,N-dimethyl-formamide / 4 h / 20 °C
View Scheme
参考文献
Xu, Lanting; Jiang, Yongwen; Ma, Dawei
Organic Letters, 2012 , vol. 14, # 4 p. 1150 - 1153
反应条件
pyridine
T=160 - 170°C; 0.5 h;
参考文献
Ashare, Ram; Mukerjee, Arya K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 1180 - 1181
反应条件
in tetrahydrofuran
T=-78 - 20°C; 29 h; ConcentrationTime;
参考文献
Nakano, Hayato; Kutsumura, Noriki; Saito, Takao
Synthesis (Germany), 2012 , vol. 44, # 20 p. 3179 - 3184
反应条件
toluene-4-sulfonic acid
Irradiation;
参考文献
Rad-Moghadam, Kurosh; Khajavi, Mohammad S.
Journal of Chemical Research - Part S, 1998 , # 11 p. 702 - 703
反应条件
1: 85 percent / 4 h / Heating
2: 51 percent / phosphorus oxychloride / CH2Cl2 / 4 h / Heating
View Scheme
参考文献
Mahindroo, Neeraj; Ahmed, Zabeer; Bhagat, Asha; Bedi, Kasturi Lal; Khajuria, Ravi Kant; Kapoor, Vijay Kumar; Dhar, Kanaya Lal
Medicinal Chemistry Research, 2005 , vol. 14, # 6 p. 347 - 368
反应条件
1: 58 percent / triethylamine / benzene
2: 65 percent / Ph3PBr2 / CH2Cl2 / 3 h / Heating
View Scheme
参考文献
Mazurkiewicz, Roman
Monatshefte fuer Chemie, 1989 , vol. 120, p. 973 - 980
反应条件
1: platinum(IV) oxide; hydrogen / ethanol / 20 °C
2: ethanol / 5 h / 0 - 20 °C
3: potassium iodide / ethanol; water / 6 h / 20 °C
4: piperidine / 20 - 50 °C
View Scheme
参考文献
Kumar, R. Arun; Maheswari, C. Uma; Ghantasala, Satheesh; Jyothi; Reddy, K. Rajender
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 2-3 p. 401 - 410
