2-硝基-N-苯基苯甲酰胺合成路线 （共 25 条）
反应条件
sodium hydroxide; zinc in methanol
15 h; Heating;
参考文献
Bird; Chng; Rama; Saeed
Synthetic Communications, 1991 , vol. 21, # 4 p. 545 - 548
反应条件
1: Sn, 6 N HCl / tetrahydrofuran / 1 h / 50 °C
2: pyridine / 1.5 h / 60 °C
View Scheme
参考文献
Ogata, Masaru; Matsumoto, Hiroshi; Shimizu, Sumio; Kida, Shiro; Wada, Toru; et al.
Journal of Medicinal Chemistry, 1986 , vol. 29, # 3 p. 417 - 423
反应条件
1,1'-bis-(diphenylphosphino)ferrocene in chlorobenzene
T=160°C; 24 h; Inert atmosphereSealed tube; Catalytic behavior; Reagent/catalystSolventTemperature;
参考文献
Wang, Huamin; Cao, Xiangxiang; Xiao, Fuhong; Liu, Saiwen; Deng, Guo-Jun
Organic Letters, 2013 , vol. 15, # 18 p. 4900 - 4903
反应条件
1,1'-bis-(diphenylphosphino)ferrocene
T=160°C; 24 h; Inert atmosphere;
参考文献
Wang, Huamin; Cao, Xiangxiang; Xiao, Fuhong; Liu, Saiwen; Deng, Guo-Jun
Organic Letters, 2013 , vol. 15, # 18 p. 4900 - 4903
反应条件
1: phosphorus pentachloride
2: petroleum ether
3: zinc dust; glacial acetic acid / 20 °C
4: beim Benzoylieren und Behandeln mit alkoh. Salzsaeure bei 20grad
View Scheme
参考文献
Shah
Journal of the Indian Institute of Science, 1924 , vol. 7, p. 217
Chem. Zentralbl., 1925 , vol. 96, # I p. 659
