4,4'-二氯二苯乙醇酸合成路线 (共 10 条)
反应条件
1: With oxygen; 1-n-butyl-3-methylimidazolium tetrafluoroborate; potassium hydroxide T=60°C; 0.333333 h; Neat (no solvent)Microwave irradiation; 2: With hydrogenchloride in water T=20°C;
参考文献
Singh, Neetu; Singh, Satish Kumar; Khanna; Singh, Krishna Nand
Tetrahedron Letters, 2011 , vol. 52, # 18 p. 2419 - 2422
反应条件
potassium hydroxide T=80°C; 6 h;
参考文献
Toda, Fumio; Tanaka, Koichi; Kagawa, Yukiko; Sakaino, Yoshiko
Chemistry Letters, 1990 , # 3 p. 373 - 376
反应条件
potassium hydroxide in ethanol 2 h; Ambient temperature;
参考文献
Beasley, Helen L.; Phongkham, Thipsavanh; Daunt, Margaret H.; Guihot, Simone L.; Skerritt, John H.
Journal of Agricultural and Food Chemistry, 1998 , vol. 46, # 8 p. 3339 - 3352
反应条件
potassium iodide in N,N-dimethyl-formamide Hg pool cathode, platinum plate anode, constant current of 2.5 nA/cm2;
参考文献
Ikeda, Yoshikazu; Manda, Eiichiro
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 6 p. 1723 - 1726
参考文献
Welch; Smith
Journal of the American Chemical Society, 1953 , vol. 75, p. 1412,1414
反应条件
1: chlorine; CCl4 / Einwirkung von Licht 2: aqueous Na2CO3 View Scheme
参考文献
Welch; Smith
Journal of the American Chemical Society, 1953 , vol. 75, p. 1412,1414
反应条件
1: diluted nitric acid 2: alcoholic potash View Scheme
参考文献
Montagne
Recueil des Travaux Chimiques des Pays-Bas, 1902 , vol. 21, p. 25
Recueil des Travaux Chimiques des Pays-Bas, 1906 , vol. 25, p. 384
反应条件
T=60.5°C; Umlagerung; Rate constant;
参考文献
Pfeil et al.
Chemische Berichte, 1956 , vol. 89, p. 1210,1225
参考文献
Voegtli; Laeuger
Helvetica Chimica Acta, 1955 , vol. 38, p. 46,63
反应条件
sodium periodate; dibenzo-18-crown-6; N-benzyl-N,N,N-triethylammonium chloride in methanol 2.1 h;
参考文献
Kore, A. R.; Sagar, A. D.; Salunkhe, M. M.
Organic Preparations and Procedures International, 1995 , vol. 27, # 3 p. 373 - 382