1-(2-硝基-1-丙烯基)萘合成路线 (共 4 条)
反应条件
N-butylamine in benzene 192 h; Heating;
参考文献
Vilches-Herrera, Marcelo; Miranda-Sepulveda, Juan; Rebolledo-Fuentes, Marco; Fierro, Angelica; Luehr, Susan; Iturriaga-Vasquez, Patricio; Cassels, Bruce K.; Reyes-Parada, Miguel
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 6 p. 2452 - 2460
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran Reflux; 2: With sodium hydroxide; water in tetrahydrofuran T=20°C; 3: With hydrogenchloride in water; isopropyl alcohol
参考文献
Vilches-Herrera, Marcelo; Miranda-Sepulveda, Juan; Rebolledo-Fuentes, Marco; Fierro, Angelica; Luehr, Susan; Iturriaga-Vasquez, Patricio; Cassels, Bruce K.; Reyes-Parada, Miguel
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 6 p. 2452 - 2460
反应条件
L-Selectridereg; in tetrahydrofuran 1.5 h;
参考文献
Mourad, M. Soubei; Varma, Rajender S.; Kabalka, George W.
Synthesis, 1985 , # 6/7 p. 654 - 656
反应条件
hydrogenchloride; potassium hydroxide
1) ether, reflux, 2) methanol, water, 0.5 h, reflux; Yield given. Multistep reaction;
参考文献
Boberg, Friedrich; Garburg, Karl-Heinz; Goerlich, Karl-Joachim; Pipereit, Eberhard; Ruhr, Maria
Liebigs Annalen der Chemie, 1985 , # 2 p. 239 - 250