in water byproducts: AgI; addn. of soln. of AgNO3 to suspn. of complex, stirring (50°C, 1 h), filtration, addn. of tenfold excess of NaCl, heating (0.5 h); cooling (4°C), filtration, washing (ice-cold H2O, EtOH, ether);
参考文献
Australian Journal of Chemistry, , vol. 48, # 4 p. 793 - 806
silver sulphate in water byproducts: AgI; Ag:Pt=1.28:0.65 molar ratio, Pt compd. added to a soln. of Ag salt, stirred overnight at 40°C in the dark, filtered, KCl (excess) added, stored for 24 h; ppt. centrifuged, washed (cold water, ethanol, diethyl ether), dried (vac.);
