N-二甲基氨基硼烷基-N-甲基甲胺合成路线 (共 17 条)
反应条件
(CH3)3N equil. react. at 140°C;
参考文献
Burg, A. B.; Randolph, C. L.
Journal of the American Chemical Society, 1951 , vol. 73, p. 953 - 957
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Gmelin Handbook: B: B-Verb.4, 3.2, page 41 - 51
参考文献
Burg, A. B.; Randolph, C. L.
Journal of the American Chemical Society, 1951 , vol. 73, p. 953 - 957
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Gmelin Handbook: B: B-Verb.4, 2.2, page 5 - 25
反应条件
T=140°C; Bei mehrtaegigem Erhitzen;
参考文献
Burg; Randolph
Journal of the American Chemical Society, 1951 , vol. 73, p. 953,956
参考文献
Gmelin Handbook: B: SVol.1, 4.10, page 238 - 241
参考文献
Z. Anorg. Chem., , vol. 257, p. 131 - 137
反应条件
in neat (no solvent) byproducts: B{N(CH3)2}3; 140°C, several days;;
参考文献
Burg, A. B.; Randolph, C. L.
Journal of the American Chemical Society, 1951 , vol. 73, p. 953 - 957
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Gmelin Handbook: B: B-Verb.14, 3.8, page 77 - 81
反应条件
HCl in diethyl ether at 0°C;
参考文献
Noeth, H.; Dorokhov, V. A.; Fritz, P.; Pfab, F.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1962 , vol. 318, p. 293 - 303
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Gmelin Handbook: B: B-Verb.4, 3.2, page 41 - 51
反应条件
transamination, boiling the educts under nitrogene, distn. of dimethylamine during the reaction; distn.;
参考文献
Niedenzu, K.; Fritz, P.; Dawson, J. W.
Inorganic Chemistry, 1964 , vol. 3, p. 1077 - 1079
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Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
反应条件
transamination, boiling the educts under nitrogene, distn. of dimethylamine during the reaction; distn.;
参考文献
Niedenzu, K.; Fritz, P.; Dawson, J. W.
Inorganic Chemistry, 1964 , vol. 3, p. 1077 - 1079
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Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
反应条件
water byproducts: H2; at room temp.;
参考文献
Gmelin Handbook: B: SVol.1, 4.10, page 238 - 241