您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
23866-67-3
合成路线
（共 24 条）
109-04-6
邻溴吡啶
+
86-74-8
咔唑
→
反应条件
23866-67-3
反应条件
copper(l) iodide; caesium carbonate in N,N-dimethyl-formamide T=220°C; 0.666667 h; Microwave irradiation;
参考文献
Kwon, Jae Kwan; Cho, Joong Hyun; Ryu, Young-Sil; Oh, Se Hwan; Yum, Eul Kgun
Tetrahedron, 2011 , vol. 67, # 26 p. 4820 - 4825
5029-67-4
2-碘吡啶
+
86-74-8
咔唑
→
反应条件
23866-67-3
反应条件
18-crown-6 ether; copper; potassium carbonate in dichlorobenzene, o- 10 h; Heating / reflux;
参考文献
Semiconductor Energy Laboratory Co., Ltd.
Patent: US2004/230061 A1, 2004 ;
Location in patent: Page/Page column 9 ;
372-48-5
2-氟吡啶
+
86-74-8
咔唑
→
反应条件
23866-67-3
反应条件
sodium hydride in N,N-dimethyl-formamide T=125 - 130°C; 1 h;
参考文献
Seki, Koh-ichi; Ohkura, Kazue; Terashima, Masanao; Kanaoka, Yuichi
Heterocycles, 1994 , vol. 37, # 2 p. 993 - 996
1256380-82-1
→
反应条件
23866-67-3
反应条件
silver(I) acetate; palladium diacetate in 1,4-dioxane T=140°C; 1 h;
参考文献
Chu, Jean-Ho; Lin, Pi-Shan; Lee, Ya-Ming; Shen, Wei-Ting; Wu, Ming-Jung
Chemistry - A European Journal, 2011 , vol. 17, # 48 p. 13613 - 13620
6631-37-4
2-苯胺基吡啶
→
反应条件
23866-67-3
+
1256380-82-1
反应条件
silver(I) acetate; palladium diacetate; dimethyl sulfoxide; p-benozquinone in 1,4-dioxane T=130 - 140°C; 48 h;
参考文献
Chu, Jean-Ho; Lin, Pi-Shan; Lee, Ya-Ming; Shen, Wei-Ting; Wu, Ming-Jung
Chemistry - A European Journal, 2011 , vol. 17, # 48 p. 13613 - 13620
5029-67-4
2-碘吡啶
→
反应条件
23866-67-3
反应条件
1: potassium tert-butylate; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether / toluene / 100 °C / Inert atmosphere 2: palladium diacetate; copper(II) bis(trifluoromethanesulfonate); silver(l) oxide / toluene / 24 h / 120 °C 3: silver(I) acetate; palladium diacetate / 1,4-dioxane / 1 h / 140 °C View Scheme
参考文献
Chu, Jean-Ho; Lin, Pi-Shan; Lee, Ya-Ming; Shen, Wei-Ting; Wu, Ming-Jung
Chemistry - A European Journal, 2011 , vol. 17, # 48 p. 13613 - 13620
1243273-04-2
→
反应条件
23866-67-3
+
1352932-75-2
反应条件
1: N-(2-deuteriophenyl)-2-aminopyridine With palladium diacetate in dichloromethane T=65 - 70°C; 4 h; 2: PhBF3(-)K(+) With silver(I) acetate; p-benozquinone in 1,4-dioxane T=110°C; 4 h;
参考文献
Chu, Jean-Ho; Lin, Pi-Shan; Lee, Ya-Ming; Shen, Wei-Ting; Wu, Ming-Jung
Chemistry - A European Journal, 2011 , vol. 17, # 48 p. 13613 - 13620
74497-02-2
→
反应条件
23866-67-3
反应条件
1: potassium tert-butylate; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether / toluene / 100 °C / Inert atmosphere 2: palladium diacetate; copper(II) bis(trifluoromethanesulfonate); silver(l) oxide / toluene / 24 h / 120 °C 3: silver(I) acetate; palladium diacetate / 1,4-dioxane / 1 h / 140 °C View Scheme
参考文献
Chu, Jean-Ho; Lin, Pi-Shan; Lee, Ya-Ming; Shen, Wei-Ting; Wu, Ming-Jung
Chemistry - A European Journal, 2011 , vol. 17, # 48 p. 13613 - 13620
6631-37-4
2-苯胺基吡啶
→
反应条件
50910-08-2
+
23866-67-3
+
1256380-82-1
反应条件
copper diacetate; palladium diacetate; p-benozquinone in N,N-dimethyl-formamide T=80 - 90°C; 4 h; Overall yield = 56 percent;
参考文献
Chu, Jean-Ho; Huang, Hao-Ping; Hsu, Wen-Ting; Chen, Shih-Tien; Wu, Ming-Jung
Organometallics, 2014 , vol. 33, # 5 p. 1190 - 1204
1243273-04-2
→
反应条件
23866-67-3
+
1256380-82-1
+
1352932-73-0
+
1352932-75-2
反应条件
silver(I) acetate; palladium diacetate; dimethyl sulfoxide; p-benozquinone in 1,4-dioxane T=130 - 140°C; 48 h;
参考文献
Chu, Jean-Ho; Lin, Pi-Shan; Lee, Ya-Ming; Shen, Wei-Ting; Wu, Ming-Jung
Chemistry - A European Journal, 2011 , vol. 17, # 48 p. 13613 - 13620
1
2
3
下一页
末页
到第
页
确定
