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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
23866-67-3
合成路线
（共 24 条）
6631-37-4
2-苯胺基吡啶
→
反应条件
23866-67-3
反应条件
1: palladium diacetate; copper(II) bis(trifluoromethanesulfonate); silver(l) oxide / toluene / 24 h / 120 °C 2: silver(I) acetate; palladium diacetate / 1,4-dioxane / 1 h / 140 °C View Scheme
参考文献
Chu, Jean-Ho; Lin, Pi-Shan; Lee, Ya-Ming; Shen, Wei-Ting; Wu, Ming-Jung
Chemistry - A European Journal, 2011 , vol. 17, # 48 p. 13613 - 13620
615-36-1
2-溴苯胺
→
反应条件
23866-67-3
反应条件
1.1: potassium tert-butylate; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether / toluene / 100 °C / Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -42 °C / Inert atmosphere 2.2: 0.5 h / Inert atmosphere 3.1: silver(I) acetate; palladium diacetate; dimethyl sulfoxide; p-benozquinone / 1,4-dioxane / 48 h / 130 - 140 °C 4.1: silver(I) acetate; palladium diacetate / 1,4-dioxane / 1 h / 140 °C View Scheme
参考文献
Chu, Jean-Ho; Lin, Pi-Shan; Lee, Ya-Ming; Shen, Wei-Ting; Wu, Ming-Jung
Chemistry - A European Journal, 2011 , vol. 17, # 48 p. 13613 - 13620
239137-40-7
→
反应条件
23866-67-3
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -42 °C / Inert atmosphere 1.2: 0.5 h / Inert atmosphere 2.1: silver(I) acetate; palladium diacetate; dimethyl sulfoxide; p-benozquinone / 1,4-dioxane / 48 h / 130 - 140 °C 3.1: silver(I) acetate; palladium diacetate / 1,4-dioxane / 1 h / 140 °C View Scheme
参考文献
Chu, Jean-Ho; Lin, Pi-Shan; Lee, Ya-Ming; Shen, Wei-Ting; Wu, Ming-Jung
Chemistry - A European Journal, 2011 , vol. 17, # 48 p. 13613 - 13620
372-48-5
2-氟吡啶
+
33650-06-5
→
反应条件
23866-67-3
反应条件
in Petroleum ether Irradiation;
参考文献
Seki, Koh-Ichi; Ohkura, Kazue; Matsuda, Kohki; Terashima, Masanao; Kanaoka, Yuichi
Chemical & Pharmaceutical Bulletin, 1988 , vol. 36, # 12 p. 4693 - 4699
5029-67-4
2-碘吡啶
→
反应条件
23866-67-3
+
1256380-82-1
反应条件
1: potassium tert-butylate; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether / toluene / 100 °C / Inert atmosphere 2: silver(I) acetate; palladium diacetate; dimethyl sulfoxide; p-benozquinone / tert-butyl alcohol / 48 h / 130 - 140 °C View Scheme
参考文献
Chu, Jean-Ho; Lin, Pi-Shan; Lee, Ya-Ming; Shen, Wei-Ting; Wu, Ming-Jung
Chemistry - A European Journal, 2011 , vol. 17, # 48 p. 13613 - 13620
5029-67-4
2-碘吡啶
→
反应条件
23866-67-3
+
1352932-75-2
反应条件
1.1: potassium tert-butylate; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether / toluene / 100 °C / Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -42 °C / Inert atmosphere 2.2: 0.5 h / Inert atmosphere 3.1: palladium diacetate / dichloromethane / 4 h / 65 - 70 °C 3.2: 4 h / 110 °C View Scheme
参考文献
Chu, Jean-Ho; Lin, Pi-Shan; Lee, Ya-Ming; Shen, Wei-Ting; Wu, Ming-Jung
Chemistry - A European Journal, 2011 , vol. 17, # 48 p. 13613 - 13620
1243273-04-2
→
反应条件
23866-67-3
反应条件
1: silver(I) acetate; palladium diacetate; dimethyl sulfoxide; p-benozquinone / 1,4-dioxane / 48 h / 130 - 140 °C 2: silver(I) acetate; palladium diacetate / 1,4-dioxane / 1 h / 140 °C View Scheme
参考文献
Chu, Jean-Ho; Lin, Pi-Shan; Lee, Ya-Ming; Shen, Wei-Ting; Wu, Ming-Jung
Chemistry - A European Journal, 2011 , vol. 17, # 48 p. 13613 - 13620
6631-37-4
2-苯胺基吡啶
+
98-80-6
苯硼酸
→
反应条件
23866-67-3
反应条件
1: palladium diacetate; copper(II) bis(trifluoromethanesulfonate); silver(l) oxide / toluene / 24 h / 120 °C 2: silver(I) acetate; palladium diacetate / 1,4-dioxane / 1 h / 140 °C View Scheme
参考文献
Chu, Jean-Ho; Lin, Pi-Shan; Lee, Ya-Ming; Shen, Wei-Ting; Wu, Ming-Jung
Chemistry - A European Journal, 2011 , vol. 17, # 48 p. 13613 - 13620
74497-02-2
→
反应条件
23866-67-3
+
1256380-82-1
反应条件
1: potassium tert-butylate; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether / toluene / 100 °C / Inert atmosphere 2: silver(I) acetate; palladium diacetate; dimethyl sulfoxide; p-benozquinone / tert-butyl alcohol / 48 h / 130 - 140 °C View Scheme
参考文献
Chu, Jean-Ho; Lin, Pi-Shan; Lee, Ya-Ming; Shen, Wei-Ting; Wu, Ming-Jung
Chemistry - A European Journal, 2011 , vol. 17, # 48 p. 13613 - 13620
615-36-1
2-溴苯胺
→
反应条件
23866-67-3
+
1352932-75-2
反应条件
1.1: potassium tert-butylate; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether / toluene / 100 °C / Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -42 °C / Inert atmosphere 2.2: 0.5 h / Inert atmosphere 3.1: palladium diacetate / dichloromethane / 4 h / 65 - 70 °C 3.2: 4 h / 110 °C View Scheme
参考文献
Chu, Jean-Ho; Lin, Pi-Shan; Lee, Ya-Ming; Shen, Wei-Ting; Wu, Ming-Jung
Chemistry - A European Journal, 2011 , vol. 17, # 48 p. 13613 - 13620
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