in neat (no solvent) Irradiation (UV/VIS); irradiation of a 1:2 molar mixt. of Mn complex and amine with UV light in a quartz vessel under Ar, 140h; crystn. of dialkylurea; filtration, refluxing crystals (EtOH), filtration, evapn.; evapn. of mother liquor of first filtration; washing (light petroleum); elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 414, # 1 p. 65 - 69
