2-甲基-3-硝基苯甲醇合成路线 （共 28 条）
反应条件
pyridine; thionyl chloride
参考文献
Gallagher, Gregory; Lavanchy, Patricia G.; Wilson, James W.; Hieble, J. Paul; DeMarinis, Robert M.
Journal of Medicinal Chemistry, 1985 , vol. 28, # 10 p. 1533 - 1536
反应条件
1: (i) PBr3, (ii) /BRN= 4652394/ 2: H2SO4 3: H2 / Pt-C View Scheme
参考文献
Askam; Keeks
Journal of the Chemical Society. Perkin transactions 1, 1969 , vol. 14, p. 1935 - 1939
反应条件
1: 100 percent / SOCl2, pyridine 2: 99 percent / ethanol; H2O 3: 97 percent / H2SO4, HOAc / H2O View Scheme
参考文献
Askam; Keeks
Journal of the Chemical Society. Perkin transactions 1, 1969 , vol. 14, p. 1935 - 1939
反应条件
1: SOCl2, pyridine View Scheme
参考文献
Gallagher, Gregory; Lavanchy, Patricia G.; Wilson, James W.; Hieble, J. Paul; DeMarinis, Robert M.
Journal of Medicinal Chemistry, 1985 , vol. 28, # 10 p. 1533 - 1536
反应条件
(i) PBr3, (ii) /BRN= 4652394/; Multistep reaction;
参考文献
Askam; Keeks
Journal of the Chemical Society. Perkin transactions 1, 1969 , vol. 14, p. 1935 - 1939
反应条件
sodium chloride in nickel monoaluminide; dichloromethane; toluene
参考文献
FMC Corporation
Patent: US4426524 A1, 1984 ;
反应条件
toluene-4-sulfonic acid in dichloromethane
Ambient temperature;
参考文献
Shin, Chung-Gi; Yamada, Yasuhiro; Hayashi, Keiichiro; Yonezawa, Yasuchika; Umemura, Kazuyuki; Tanji, Tsuyoshi; Yoshimura, Juji
Heterocycles, 1996 , vol. 43, # 4 p. 891 - 898
反应条件
phosphorus tribromide in diethyl ether
T=50°C; 1 h;
参考文献
Mueller, Michael A.; Gaplovsky, Martin; Wirz, Jakob; Woggon, Wolf-D.
Helvetica Chimica Acta, 2006 , vol. 89, # 12 p. 2987 - 3001
