titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; alpha,alpha-dimethylbenzyl hydroperoxide in dichloromethane
T=-23°C; further reag.: t-BuOOH; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Colonna, Stefano; Gaggero, Nicoletta; Manfredi, Amedea; Casella, Luigi; Gullotti, Michele
Journal of the Chemical Society, Chemical Communications, 1988 , # 22 p. 1451 - 1452
alpha,alpha-dimethylbenzyl hydroperoxide; 4 A molecular sieve; titanium(IV) isopropylate; (3S,4S)-2,2,5,5-tetramethyl-3,4-hexanediol in toluene
T=-20°C; Oxidation; 60 h; Title compound not separated from byproducts;
参考文献
Yamanoi, Yoshinori; Imamoto, Tsuneo
Journal of Organic Chemistry, 1997 , vol. 62, # 24 p. 8560 - 8564
Holmes; Ingold; Ingold
Journal of the Chemical Society, 1926 , p. 1689
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Ingold; Ingold
Journal of the Chemical Society, 1926 , p. 3093
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Pollard; Robinson
Journal of the Chemical Society, 1926 , p. 3091 Anm.