(4-甲氧基-苯基)-对甲苯-甲酮合成路线 (共 63 条)
反应条件
potassium 12-tungstocobalt(III)ate; sodium tartrate buffer in water pH=4.0; 48 h;
参考文献
Bietti, Massimo; Lanzalunga, Osvaldo
Journal of Organic Chemistry, 2002 , vol. 67, # 8 p. 2632 - 2638
反应条件
dichloro bis(acetonitrile) palladium(II) in tetrahydrofuran T=55°C; 16 h;
参考文献
Fausett, Bryan W.; Liebeskind, Lanny S.
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4851 - 4853
反应条件
Cp2Fe in benzene-d6 byproducts: toluene, H2; under N2, standard Schlenk techniques; in NMR tube; C6D6 added to mixt. of Rh complex and Cp2Fe (small amt.); warmed at 55°C for 5 min; aldehyde (1.5 equiv.) added; heated at 85°C (oil bath) for 80 min; not isolated; monitored by (1)H NMR spectra;
参考文献
Krug, Christopher; Hartwig, John F.
Journal of the American Chemical Society, 2002 , vol. 124, # 8 p. 1674 - 1679
反应条件
tributyl-amine in 1-methyl-pyrrolidin-2-one T=80°C; 4 h; Schlenk techniqueInert atmosphere;
参考文献
Zhao, Hong; Yin, Lin; Cai, Mingzhong
European Journal of Organic Chemistry, 2013 , # 7 p. 1337 - 1345
反应条件
dichloro bis(acetonitrile) palladium(II) in tetrahydrofuran T=55°C; 16 h;
参考文献
Fausett, Bryan W.; Liebeskind, Lanny S.
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4851 - 4853
反应条件
palladium diacetate; potassium carbonate in methoxybenzene T=140°C; Suzuki coupling; 12 h;
参考文献
Jafarpour, Farnaz; Rashidi-Ranjbar, Parviz.; Kashani, Asieh Otaredi
European Journal of Organic Chemistry, 2011 , # 11 p. 2128 - 2132
反应条件
tetrakis(triphenylphosphine) palladium(0); water; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline in N,N-dimethyl-formamide T=60°C; 30 h; Inert atmosphere;
参考文献
Kwon, Young Bum; Choi, Bo Ram; Lee, Seung Hwan; Seo, Jin-Soo; Yoon, Cheol Min
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 9 p. 2672 - 2674
反应条件
phosphorus pentoxide on alumina in 1,2-dichloro-ethane Friedel-Crafts acylation; 5 h; Reflux; chemoselective reaction;
参考文献
Hajipour, Abdol R.; Zarei, Amin; Khazdooz, Leila; Ruoho, Arnold E.
Synthetic Communications, 2009 , vol. 39, # 15 p. 2702 - 2722
反应条件
1,10-phenanthroline; palladium(II) oxide hydrate; trifluoroacetic acid in 1,4-dioxane; water T=110°C; 20 h; AirClosed vessel;
参考文献
Liu, Jing; Zhou, Xianya; Rao, Honghua; Xiao, Fuhong; Li, Chao-Jun; Deng, Guo-Jun
Chemistry - A European Journal, 2011 , vol. 17, # 29 p. 7996 - 7999
反应条件
1,10-phenanthroline; palladium(II) oxide hydrate; trifluoroacetic acid in 1,4-dioxane; water T=110°C; 20 h; AirClosed vessel;
参考文献
Liu, Jing; Zhou, Xianya; Rao, Honghua; Xiao, Fuhong; Li, Chao-Jun; Deng, Guo-Jun
Chemistry - A European Journal, 2011 , vol. 17, # 29 p. 7996 - 7999