13H-二苯并(a,i)芴合成路线 （共 19 条）
反应条件
T=800°C; 0.583333 h; presence of reagent: phosphoric acid; Title compound not separated from byproducts;
参考文献
Regimbald-Krnel, Michele; Wentrup, Curt
Journal of Organic Chemistry, 1998 , vol. 63, # 23 p. 8417 - 8423
反应条件
2: zinc; hydrochloric acid; glacial acetic acid
View Scheme
参考文献
Tschitschibabin; Magidson
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1914 , vol. 46, p. 1393
Chem. Zentralbl., 1915 , vol. 86, # I p. 1123
反应条件
hydrogen iodide; acetic acid
参考文献
Wanscheidt
Chemische Berichte, 1926 , vol. 59, p. 2099
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1926 , vol. 58, p. 257,262
Chem. Zentralbl., 1927 , vol. 98, # I p. 92
反应条件
phosphoric acid
T=240°C; 2.5 h; other reagent: AlCl3, reagent absence, solvents: naphthalene, benzene, CS2, other temperature and time; Product distributionMechanism;
参考文献
Regimbald-Krnel, Michele; Wentrup, Curt
Journal of Organic Chemistry, 1998 , vol. 63, # 23 p. 8417 - 8423
反应条件
1: aq. H2SO4
2: N2H4*H2O, KOH / 160 - 195 °C
View Scheme
参考文献
Rao,R.A.; Rao,R.R.
Indian Journal of Chemistry, 1968 , vol. 6, p. 130 - 131
反应条件
T=-40 - 18°C; other reactant: diphenylcarbinol, other reagent: phosphoric acid, other temperature; MechanismProduct distribution;
参考文献
Regimbald-Krnel, Michele; Wentrup, Curt
Journal of Organic Chemistry, 1998 , vol. 63, # 23 p. 8417 - 8423
反应条件
T=120 - 145°C; Erhitzen des Reaktionsprodukts mit Zink-Pulver,ZnCl2 und NaCl;
参考文献
Buu-Hoi; Cagniant
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1943 , vol. 216, p. 299
反应条件
(i), (ii) HI, AcOH; Multistep reaction;
参考文献
Kuhn,R.; Rewicki,D.
Justus Liebigs Annalen der Chemie, 1967 , vol. 704, p. 9 - 14
反应条件
1: oxygen; 18-crown-6 ether / benzene
2: polyphosphoric acid / 1 h / 160 °C / |Inert atmosphere
View Scheme
参考文献
Mala'Bi, Tahani; Pogodin, Sergey; Cohen, Shmuel; Agranat, Israel
RSC Advances, 2013 , vol. 3, # 44 p. 21797 - 21810
