1.1: 99 percent / PDC / CH2Cl2 / 6 h 2.1: nBuLi / hexane; tetrahydrofuran / 5 h / -78 - 0 °C 2.2: 73 percent / tetrahydrofuran; hexane / 5 h / 20 °C 3.1: nBu4NF*3H2O / tetrahydrofuran / 23 h 4.1: 20 mg / AG 50W-X4 resin / methanol / 24 h View Scheme
参考文献
Perez Sestelo, Jose; Cornella, Ivan; de Una, Olga; Mourino, Antonio; Sarandeses, Luis A
Chemistry (Weinheim an der Bergstrasse, Germany), 2002 , vol. 8, # 12 p. 2747 - 2752
1.1: 99 percent / PDC / CH2Cl2 / 6 h
2.1: nBuLi / hexane; tetrahydrofuran / 5 h / -78 - 0 °C
2.2: 92 percent / tetrahydrofuran; hexane / 5 h / 20 °C
3.1: nBu4NF*3H2O / tetrahydrofuran / 22 h
4.1: AG 50W-X4 resin / methanol / 22 h
View Scheme
参考文献
Perez Sestelo, Jose; Cornella, Ivan; de Una, Olga; Mourino, Antonio; Sarandeses, Luis A
Chemistry (Weinheim an der Bergstrasse, Germany), 2002 , vol. 8, # 12 p. 2747 - 2752
