1,13-二氮杂-21-冠醚-7合成路线 （共 12 条）
反应条件
1: Et3N 2: B2H6 3: (i) aq. HCl, (ii) ion-exchange resin <OH- form> View Scheme
参考文献
Dietrich,B. et al.
Tetrahedron, 1973 , vol. 29, p. 1629 - 1645
反应条件
potassium tert-butylate in tetrahydrofuran
1) r.t., 16 h; 2) 65 deg C, 2 h;
参考文献
Jong, F. de; Zon, A. van; Reinhoudt, D. N.; Torny, G. J.; Tomassen, H. P. M.
Recueil: Journal of the Royal Netherlands Chemical Society, 1983 , vol. 102, # 3 p. 164 - 173
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
20 h; Heating;
参考文献
Luk'yanenko, N.G.; Basok, S.S.; Filonova, L.K.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, p. 1562 - 1571
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 8 p. 1731 - 1742
反应条件
potassium carbonate in acetonitrile
48 h; Heating;
参考文献
Krakowiak, Krzysztof E.; Maas, Garren E.; Bradshaw, Jerald S.; Hathaway, Jon K.; Izatt, Reed M.
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 1 p. 179 - 182
反应条件
lithium aluminium tetrahydride
参考文献
Dietrich,B. et al.
Tetrahedron, 1973 , vol. 29, p. 1629 - 1645
反应条件
potassium carbonate in acetonitrile
48 h; Heating;
参考文献
Krakowiak, Krzysztof E.; Maas, Garren E.; Bradshaw, Jerald S.; Hathaway, Jon K.; Izatt, Reed M.
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 1 p. 179 - 182
反应条件
1: 82 percent / tetrabutylammonium iodide, sodium hydroxide (50 percent) / toluene; H2O / 9 h / Heating
2: 45 percent / lithium aluminum hydride / tetrahydrofuran / 20 h / Heating
View Scheme
参考文献
Luk'yanenko, N.G.; Basok, S.S.; Filonova, L.K.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, p. 1562 - 1571
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 8 p. 1731 - 1742
反应条件
1: 82 percent / tetrabutylammonium iodide, sodium hydroxide (50 percent) / toluene; H2O / 9 h / Heating
2: 45 percent / lithium aluminum hydride / tetrahydrofuran / 20 h / Heating
View Scheme
参考文献
Luk'yanenko, N.G.; Basok, S.S.; Filonova, L.K.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, p. 1562 - 1571
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 8 p. 1731 - 1742
反应条件
1: 82 percent / tetrabutylammonium iodide, sodium hydroxide (50 percent) / toluene; H2O / 9 h / Heating
2: 45 percent / lithium aluminum hydride / tetrahydrofuran / 20 h / Heating
View Scheme
参考文献
Luk'yanenko, N.G.; Basok, S.S.; Filonova, L.K.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, p. 1562 - 1571
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 8 p. 1731 - 1742
反应条件
1: 82 percent / tetrabutylammonium iodide, sodium hydroxide (50 percent) / toluene; H2O / 9 h / Heating
2: 45 percent / lithium aluminum hydride / tetrahydrofuran / 20 h / Heating
View Scheme
参考文献
Luk'yanenko, N.G.; Basok, S.S.; Filonova, L.K.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, p. 1562 - 1571
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 8 p. 1731 - 1742
